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US 2009/0020407 A1Published application
Method for producing pure xylylenediamine (xda)
AssigneeBASF SE
InventorsRandolf Hugo, Kirsten Dahmen, Sabine Huber
Life of this patent
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Abstract
A process comprising: continuously distilling a crude xylylenediamine in a column to form a pure xylylenediamine and a bottom product, wherein the column comprises a distillation column having a side draw and the distillation column is operated under a reduced pressure and a bottom temperature of 185° C. or less; drawing off the pure xylylenediamine from the side draw; evaporatively concentrating the bottom product of the distillation column in an additional evaporation stage to form a condensate; and returning the condensate into the distillation column
Claims18
1-18. (canceled)
A process comprising:
- continuously distilling a crude xylylenediamine in a column to form a pure xylylenediamine and a bottom product, wherein the column comprises a distillation column having a side draw and the distillation column is operated under a reduced pressure and a bottom temperature of 185° C. or less,
- drawing off the pure xylylenediamine from the side draw,
- evaporatively concentrating the bottom product of the distillation column in an additional evaporation stage to form a condensate, and
- returning the condensate into the distillation column.
1 more element
Dependencies are inferred from the claim text.