CRYSTALLINE K-252b, SODIUM SALT, HYDRATE
AssigneeAbbott Laboratories
InventorRodger F. Henry
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Abstract
A crystalline (9S-(9α,10β,12α))-2,3,9,10,11,12-hexahydro-10-hydroxy-10-(carboxylate)-9-methyl-9,12-epoxy-1H-diindolo[1,2,3-fg:3′,2′,1′-kl]pyrrolo[3,4-i][1,6]benzodiazocin-1-one hydrate and ways to make it are disclosed.
Claims1
Crystalline (9S-(9α,10β,12α))-2,3,9,10,11,12-hexahydro-10-hydroxy-10-(carboxylate)-9-methyl-9,12-epoxy-1H-diindolo[1,2,3-fg:3′,2′,1′-kl]pyrrolo[3,4-i][1,6]benzodiazocin-1-one hydrate characterized in the monoclinic crystal system and C2 space group, when measured at about −100° C. with Mo—Kα radiation, by lattice parameters a, b and c of 27.28 ű0.01 Å, 9.473 ű0.005 Å and 9.052 ű0.005 Å, respectively, and β of 104.2181°±0.009.
Dependencies are inferred from the claim text.