Amorphous submicron particles
AssigneeEvonik Degussa GmbH
InventorsKarl Meier, Ulrich Brinkmann, Christian Panz, Doris Misselich, Christian Goetz
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Abstract
A process for milling amorphous solids using a milling apparatus can result in particles having a median particle diameter d50 of <1.5 μm. The process includes: operating a mill in a milling phase with an operating medium selected from the group consisting of gas, vapor, steam, a gas containing steam and mixtures thereof, and heating a milling chamber in a heat-up phase before the actual operation with the operating medium in such a way that a temperature in the milling chamber, the mill exit or both, is higher than a dew point of the operating medium.
Claims25
A process for milling amorphous solids using a milling apparatus, comprising:
- operating a mill in a milling phase with an operating medium selected from the group consisting of gas, vapor, steam, a gas containing steam and mixtures thereof, and
- heating a milling chamber in a heat-up phase before the actual operation with the operating medium in such a way that a temperature in the milling chamber, the mill exit or both, is higher than a dew point of the operating medium.
Amorphous pulverulent solids having a median particle size d50 (TEM) of <1.5 μm and/or a d90 value (TEM) of <2 μm and/or a d99 value (TEM) of <2 μm.
Dependencies are inferred from the claim text.