Nanoscale rutile or nanoscale oxide and method for producing the same
AssigneeItN Nanovation AG
InventorRalph Nonninger
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AssigneeItN Nanovation AG
InventorRalph Nonninger
Estimating the term…
The invention relates to nanoscale rutile or oxide powder that is obtained by producing amorphous TiO2 by mixing an alcoholic solution with a titanium alcoholate and with an aluminium alcohalate and adding water and acid. The amorphous, aluminum-containing TiO2 is isolated by removing the solvent, and is redispersed in water in the presence of a tin salt. Thermal or hydrothermal post-processing yields rutile or oxide that can be redispersed to primary particle size. The n-rutile or the obtained oxide having a primary particle size ranging between 5 and 20 nm can be incorporated into all organic matrices so that they remain transparent. Photocatalytic activity is suppressed by lattice doping with trivalent ions. If the amorphous precursor is redispersed in alcohol, or not isolated, but immediately crystallized, an anatase is obtained that can be redispersed to primary particle size. A variation of the alcoholates allows production of the following components: ZrO2, ZnO, SnO2, ATO, In2O3, ITO, Y2O3, BaO, CaO, MgO, CeO2, and BaTiO.
1-10. (canceled)
A method for producing a nanoscale rutile or oxide, the method comprising the steps of:
A method for producing a nanoscale rutile or oxide, the method comprising the steps of:
The method of claim 10, wherein the nanoscale rutile or the nanoscale oxide contains between 0.1 mol % and 0.5 mol % of aluminum.
A rutile which is completely redispersed to a primary particle size in H2O or an organic solution, the rutile having a primary particle size between 5 nm and 10 nm, wherein the rutile is lattice-doped with at least one of tin, sodium or ammonium atoms.
N—ZrO2, n-BaTiO3 or anatas, wherein the n-ZrO2, the n-BaTiO3, or the anatas is completely redispersed to primary particle size in H2O or an organic solution, the anatas, the n-ZrO2, the n-BaTiO3 having a primary particle size of between 3 nm and 10 nm.
Dependencies are inferred from the claim text.