# US 2004/0168978 A1 · Method and apparatus for recirculating tangential separation system

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- Number: US 2004/0168978 A1
- Document ID: US20040168978A1
- Status: Published application
- Kind: A1
- Application number: 10/474,995
- Filed: 2004-04-26
- Published: 2004-09-02
- Earliest claimed: 2001-04-18
- Inventors: Buddy Don Gray
- Web page: https://patentgrep.com/patent/US20040168978A1

## CPC

- B01D 61/025: {Reverse osmosis; Hyperfiltration}
- B01D 61/081: {used at home, e.g. kitchen}
- B01D 61/12: Controlling or regulating
- B01D 61/14: Ultrafiltration; Microfiltration
- B01D 61/22: Controlling or regulating
- B01D 65/02: Membrane cleaning or sterilisation {; Membrane regeneration}
- C02F 1/441: {by reverse osmosis}
- B01D 2321/2025: Tangential inlet
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- C02F: TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE (separation in general B01D; special arrangements on waterborne vessels of installations for treating water, waste water or sewage, e.g. for producing fresh water, B63J; adding materials to water to prevent corrosion C23F; treating radioactively-contaminated liquids G21F9/04; regeneration of reactants for recirculation into processes, see the relevant places for the processes)

## Abstract

A method of separating a mixture into a plurality of more concentrated products utilizing recirculation and concentration of one product so as to extract a substantially large fraction of another product from the mixture; and the apparatus utilizing the present method in a system, such as a reverse osmosis system, capable of very high recovery rates, efficient power usage, and long component life. Substantially 100% of the concentrate product exiting a tangential separation device, such as a reverse osmosis filtering device, recirculates until the concentration of the concentrate reaches a predetermined level, at which time the concentrate is purged from the system and a new cycle begins. This achieves recovery rates in RO-based water purification systems from around 70% for feed water with 1,000 ppm of total dissolved solids to around 97% for feed water with 100 ppm of total dissolved solids. The method and apparatus also provide for automated cleaning and maintenance of the separation and filtration elements, thus optimizing the life of the components.

## Claims

### Claim 1

A method of separating a feed mixture into a plurality of products in a filter system, comprising:
passing the feed mixture through a separation device to separate the feed mixture into a first product and a second product that are purer and more concentrated, respectively, than the feed mixture;
mixing the second product with the flow of the feed mixture prior to its entry into the separation device;
continuing the separating and mixing steps until the second product reaches a predetermined concentrate level;
purging the concentrated second product when the predetermined concentrate level is reached; and
repeating the separating, mixing, and purging steps.

### Claim 2 (depends on 1)

The method of claim 1 comprising heating the second product prior to mixing with the feed mixture.

### Claim 3 (depends on 1)

The method of claim 1 wherein the mixture of the second product and the feed mixture are heated prior to the separating step.

### Claim 4 (depends on 1)

The method of claim 1 further comprising introducing a cleaner to clean the system.

### Claim 5

A feed fluid treatment apparatus, comprising:
a tangential filtration device having an inlet to receive the feed fluid and configured to separate the feed fluid into a permeate fluid that is substantially free from contaminants, and a concentrate fluid wherein the contaminants removed from the feed fluid are concentrated;
a concentrate fluid circuit configured to receive the concentrate fluid exiting the tangential filtration device and to circulate the concentrate fluid back to the inlet of the tangential filtration device, and to mix the circulating concentrate fluid with the feed fluid prior to the tangential filtration device, effectively increasing the concentration of the concentrate fluid;
a monitoring device configured to monitor the concentrate fluid and initiate purging of the apparatus when the predetermined concentration of the concentrate fluid is reached;
a purge system configured to purge the apparatus of the concentrate fluid when the predetermined concentration of the concentrate fluid is reached;
an inlet configured to admit feed fluid to be added to the circulating concentrate fluid to replace the amount of permeate fluid permeating said tangential filtration device and to replenish the apparatus with fresh feed fluid as the apparatus is purged of the concentrated circulating concentrate fluid.

### Claim 6 (depends on 5)

The fluid treatment apparatus of claim 5 wherein the concentrate fluid circuit further comprises a filtration device configured to trap a portion of the concentrate fluid, effectively lowering the concentration of the concentrate fluid.

### Claim 7 (depends on 6)

The fluid treatment apparatus of claim 6 wherein the filtration device further comprises a purge device whereby at least a portion of the contaminants trapped by the filtration device are purged out of the apparatus to effectively extend the life and maintain the performance of the filtration device.

### Claim 8 (depends on 6)

The fluid treatment apparatus of claim 6 further comprising a process device cooperating with the filtration device to cause the filtration device to trap materials that would normally pass through the filtration device.

### Claim 9 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a process device configured to cause the tangential filtration device, after being in use, to substantially regain prior performance.

### Claim 10 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a process device configured to remove from the feed fluid materials that are ruinous to the tangential filtration device.

### Claim 11 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a process device configured to remove contaminants that permeate the tangential filtration device and pass into the permeate fluid, and which are a contaminant to said permeate fluid.

### Claim 12 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a process device configured to input energy, preferably from a waste source, into the feed fluid to cause an increase in the performance of the tangential filtration device.

### Claim 13 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a monitoring device configured to monitor the concentrate in the permeate fluid.

### Claim 14 (depends on 5)

The fluid treatment apparatus of claim 5, further comprising a storage apparatus configured to store the permeate fluid.

### Claim 15 (depends on 14)

The fluid treatment apparatus of claim 14, further comprising a controller for starting and stopping processing cycles based on the contents of said storage apparatus.

### Claim 16 (depends on 14)

The fluid treatment apparatus of claim 14, further comprising a pressurization device to pressurize the permeate fluid.

### Claim 17 (depends on 14)

The fluid treatment apparatus of claim 14, further comprising a disinfecting device configured to remove microbial contamination from the permeate fluid.

### Claim 18 (depends on 14)

The fluid treatment apparatus of claim 14, further comprising a monitoring means whereby the quality of said permeate fluid is caused to be monitored; and
a controlling means whereby permeate fluid that exceeds a predetermined contaminant level is prevented from entering said storage means.

### Claim 20

A filtration method, comprising:
filtering raw water through a reverse osmosis filter system into permeate fluid and concentrate fluid;
recirculating the concentrate fluid to the raw water prior to the reverse osmosis filter device; and
purging the reverse osmosis filter system with permeate fluid when the concentrate fluid reaches a predetermined concentrate level.

### Claim 21 (depends on 20)

The method of claim 20, comprising storing the permeate fluid in a pressurized tank.

### Claim 22 (depends on 20)

The method of claim 20, comprising introducing a cleaning solution into the raw water to clean at least the reverse osmosis filter system and then purging the cleaning solution from at least the reverse osmosis filter system.

### Claim 23 (depends on 20)

The method of claim 20, comprising using an anti-microbial UV light to further filter the concentrate fluid.

### Claim 24

A filtration device, comprising:
a raw water inlet to receive raw water;
a reverse osmosis filtration system configured to filter the raw water into permeate fluid and concentrate fluid;
a recirculation system coupled to the reverse osmosis filtration system to receive the concentrate fluid and mix the same with the raw water prior to the reverse osmosis filtration system;
a delivery system configured to receive the permeate fluid and deliver final product to a product outlet.

### Claim 25 (depends on 24)

The device of claim 24, further comprising a cleaning circuit coupled to the reverse osmosis filtration system.

### Claim 26 (depends on 24)

The device of claim 24, comprising a purge line coupled between the delivery system and the reverse osmosis filtration system.
