Process for recovering and purifying caprolactam from an organic solvent
AssigneeDsm IP Assets B.V.
InventorsMaria Louisa Christina Dsinter-De Hondt, Joannes Albertus Wilhelmus Lemmens
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AssigneeDsm IP Assets B.V.
InventorsMaria Louisa Christina Dsinter-De Hondt, Joannes Albertus Wilhelmus Lemmens
Estimating the term…
Process for recovering caprolactam from a solution comprising caprolactam dissolved in an organic solvent, said process comprising: a) washing the solution with water or an aqueous alkaline solution, resulting in a washed solution comprising caprolactam and organic solvent and in a washing residue, b) evaporating organic solvent from the washed solution, resulting in caprolactam product, c) optionally, hydrogenating the caprolactam product, d) optionally, evaporating water from the caprolactam product, e) distilling the caprolactam product to recover caprolactam and a distillation residue, f) extracting the distillation residue with an organic solvent in the presence of water to obtain (i) an extract comprising caprolactam dissolved in organic solvent and (ii) an aqueous effluent, and g) recycling the extract to step a) or b).
Process for recovering caprolactam from a solution comprising caprolactam dissolved in an organic solvent, said process comprising:
Process according to any one of claims 14, wherein the organic solvent for the caprolactam is the same as the organic solvent for extracting the residue(s).
Dependencies are inferred from the claim text.