Method for continuous production of polyesters or copolyesters
AssigneeZimmer, Inc.
InventorsFritz Wilhelm, Michael Reisen
Life of this patent
Estimating the term…
Loading patent…
AssigneeZimmer, Inc.
InventorsFritz Wilhelm, Michael Reisen
Estimating the term…
Process for producing polyesters and copolyesters, wherein a continuous esterification of dicarboxylic esters and diols or a continuous transesterification of dicarboxylic esters with diols is effected in “n” reaction pressure stages connected in series, the pressure in the first reaction pressure stage is higher than that of the remaining reaction pressure stages, and successively decreases from reaction pressure stage to succeeding reaction pressure stage, the combined vapor flows of the individual reaction pressure stages are rectified in a rectifying column, and the diol component obtained at the bottom of the rectifying column is recirculated at least to the first reaction pressure stage, and wherein at least the last reaction pressure stage operates at a vacuum, the pressure in the rectifying column is greater than that of the last reaction pressure stage, and the vapors discharged from the last reaction pressure stage are condensed to the pressure existing in the rectifying column.
A process of producing polyesters and copolyesters by continuous esterification of dicarboxylic esters and diols or by continuous transesterification of dicarboxylic esters with diols in n reaction pressure stages (2, 4, 32, 34, 36) connected in series., wherein the pressure existing in the first reaction pressure stage (2, 32), which is higher as compared to the remaining reaction pressure stages (4, 34, 36), successively decreases from reaction pressure stage to reaction pressure stage, the combined vapor flows of the individual reaction pressure stages ate introduced into a rectifying column (12, 47) and rectified, and the diol component obtained at the bottom of the rectifying column is recirculated at least to the first reaction pressure stage, characterized in that at least the last reaction pressure stage has a vacuum, the pressure in the rectifying column (12, 47) is larger than in the last reaction pressure stage, and the vapors discharged from the last reaction pressure stage are condensed to the pressure existing in the rectifying column.
Dependencies are inferred from the claim text.