Sequentially cross-linked polyethylene
AssigneeHowmedica Osteonics Corp.
InventorsAiguo Wang, John H. Dumbleton
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AssigneeHowmedica Osteonics Corp.
InventorsAiguo Wang, John H. Dumbleton
Estimating the term…
A method of producing an improved polyethylene, especially an ultra-high molecular weight polyethylene utilizes a sequential irradiation and annealing process to form a highly cross-linked polyethylene material. The use of sequential irradiation followed by sequential annealing after each irradiation allows each dose of irradiation in the series of doses to be relatively low while achieving a total dose which is sufficiently high to cross-link the material. The process may either be applied to a preformed material such as a rod or bar or sheet made from polyethylene resin or may be applied to a finished polyethylene part. If applied to a finished polyethylene part, the irradiation and annealing must be accomplished with the polyethylene material not in contact with oxygen at a concentration greater than 1% oxygen volume by volume. When applied to a preform, such as a rod, the annealing of the bulk polymer part of the rod from which the finished part is made must take place on the rod before the implant is machined therefrom and exposed to oxygen.
A preformed material for subsequent production of a medical implant with improved wear resistance comprising a polyethylene cross-linked at least twice by irradiation and thermally treated by annealing after each irradiation.
A method for increasing the wear resistance of a preformed polyethylene comprising:
The method as set forth in claim 29 wherein the annealing takes place between 110° C. and 135° C.
The method for increasing the wear resistance as set forth in claim 23, wherein said material is heated for at least about 4 hours.
A medical device comprising a polyethylene material irradiated at least two times and annealed at a temperature lower than the melting point of the material after each irradiation.
Dependencies are inferred from the claim text.