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US 2003/0158410 A1Published application
Preparation of diketopyrrolopyrrole pigments
AssigneeClariant International Ltd.
InventorsUwe Nickel, Leonhard Unverdorben, Joachim Weber, Erwin Dietz, Juergen Patzlaff
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Abstract
A process for preparing diketopyrrolopyrrole pigments comprises conducting the elementary steps of pigment synthesis (reaction and hydrolysis) in a miniaturized continuous reactor.
Claims13
1) A process for preparing 1,4-diketopyrrolo[3,4-c]pyrrole pigments of the formula (I),
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- where R1 and R2 are identical or different and are each an unsubstituted or substituted isocyclic or heterocyclic aromatic radical, by reaction of a succinic diester with a nitrile of the formula (II)
- R1—CN (II)
- or of the formula (III)
- R2—CN (III)
- or with a mixture of these nitriles, in an organic solvent and in the presence of a strong base, and subsequent hydrolysis of the resultant salt of the diketopyrrolopyrrole pigment, which comprises conducting the reaction, or the hydrolysis, or the reaction and the hydrolysis, in a microreactor.
3 more elements
Dependencies are inferred from the claim text.