Method for producing 2,3-dichloro-1-propahol and epichlorohyrin

Abstract

Methods for continuously producing 2,3-dichloro-1-propanol (2,3-DCH) and epichlorohydrin in high yields and in a stabel manner for a long time are disclosed. In a method where allyl alcohol is chorinated in a hyrochloric acid solution and the reaction solution is introduced into a degassing tower to release hydrogen chloride and 2,3-DCH is obtained from the remaining solution, the concentraton of chlorine in the reaction mixture to be introduced into the degassing tower is maintaining to 0.015 g/ml or less and/or the partial pressure of chlorine gas in the reactor immediately before the degassing tower to 0.08 MPa or less, by monitoring and/or the partial pressure of chlorine gas in the reactor immediately before the degassing tower to 0.08 MPa or less, by monitoring and/or controlling the chlorine concentration of a solution at the outlet of the reactor immediately before the degassing tower and/or the partial pressure of chlorine gas present in the gas phase section of the reactor and the flow rate of chlorine gas immediately before the degassing tower.

Dependencies are inferred from the claim text.