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US 2003/0116759 A1Published application
Anthracene compound and chemiluminescent composition comprising the same
AssigneeMyung-Sook Yeom
InventorsKoon Ha Park, Yong Fan Kim, Min Seob Park
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Abstract
The present invention discloses an anthracene compound represented by the following formula 4 and chemiluminescent composition comprising the compound: 1 wherein R is an alkyl group having 1-8 carbon atoms, and X1 and X2 are independently hydrogen or halogen.
Claims17
An anthracene compound represented by the following formula(4):
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- wherein R is an alkyl group having 1-8 carbon atoms, X1 and X2 are independently hydrogen or halogen.
A preparation method of an anthracene compound comprising:
- refluxing a compound of the following formula(11) with magnesium metal in an organic solvent and cooling the refluxed solution, thereby obtaining a compound of the following formula(12);
- mixing the obtained compound of the formula(12) and anthraquinone of the following formula(13) in an organic solvent, refluxing the resulting solution, adding an aqueous acid solution to the resulting solution, extracting an organic phase, and distilling the extracted organic phase, thereby obtaining a brown solution of the following formula(14);
- and
- reacting acetic acid and a catalyst with the brown solution, thereby obtaining a compound of the formula(4).
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- wherein R is an alkyl group having 1-8 carbon atoms, and X is halogen.
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- wherein R is an alkyl group having 1-8 carbon atoms, and X is halogen.
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- wherein X1 and X2 are independently hydrogen or halogen.
- 31
- wherein R is an alkyl group having 1-8 carbon atoms, and X1 and X2 are independently hydrogen or halogen.
- 32
- wherein R is an alkyl group having 1-8 carbon atoms, and X1 and X2 are independently hydrogen or halogen.
11 more elements
Dependencies are inferred from the claim text.