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US 2002/0165397 A1Published application
2-Pyridylsilane, processes for producing and using the same
AssigneeSumitomo Chemical Company, Limited
InventorsJunichi Yoshida, Kenichiro Itami, Seiji Suga
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Abstract
The present invention provides a compound which can be purified by conventional acid/base extraction. There is disclosed 2-pyridylsilane of formula (1): 1 wherein R1 represents an alkyl group, etc, R2 and R3 represent an alkyl group, an alkoxy group, etc, R4, R5, R6 and R7 represent a hydrogen atom, a halogen atom, an alkyl group, etc.
Claims2
A method for liquid-liquid phase extraction of a compound in liquid phase combinatorial synthesis, which comprises:
- (a) subjecting a compound introduced with a 2-pyridylsilylmethylene group to a transformation reaction or reactions in liquid phase combinatorial synthesis to form a desirably modified or transformed compound,
- (b) subjecting the resulting reaction mixture containing a so transformed compound to liquid-liquid phase extraction between an organic phase and acidic aqueous phase resulting from the reaction mixture obtained in step (a) and an acidic aqueous solution and optionally an organic hydrophobic solvent to obtain an acidic aqueous phase containing the transformed compound by phase separation, and
- (c) liberating the transformed compound in the separated acidic aqueous phase by adding an alkali and extracting the liberated compound with an organic hydrophobic solvent to obtain an organic phase containing the liberated transformed compound by phase separation.
Dependencies are inferred from the claim text.