Method for producing expandable graphite intercalation compounds using phosphoric acids, and graphite foil
AssigneeSGL Technik GmbH
InventorsOswin Ottinger, Hubert Malik
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Abstract
A method for producing expandable graphite intercalation compounds uses a thermal polyphosphoric acid which is added to an intercalation agent or to graphite. Preferably, the thermal polyphosphoric acid is used in a mixture with red, fuming nitric acid. Products produced from the graphite intercalation compounds through the expanded graphite stage, such as graphite foils, graphite laminates or graphite seals, have a comparatively high fluid tightness, are relatively resistant to oxidative attack, and can have comparatively high strengths. A further advantage is a good handling ability of the thermal polyphosphoric acids. A graphite foil is also provided.
Claims43
A method for producing an expandable graphite intercalation compound, which comprises:
- reacting crystalline graphite particles having a laminar structure, in a temperature range from −10° C. to +80° C., without an additional supply of water, with a reaction mixture formed of at least one strong concentrated acid, an oxidizing agent for oxidizing the graphite, and a thermal polyphosphoric acid.
Dependencies are inferred from the claim text.