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US 12,752,249 B2Granted
Preparation method of high-efficiency gel for seawater desalination
AssigneeShanghai Maritime University
InventorsYaohua Dong, Lihua Dong, Lin Ren
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Abstract
The preparation method of the high-efficiency gel of the present invention adopts directional freezing technology and carnauba wax assisted normal pressure drying aerogel, and the aerogel has lower density, uniform and stable porous structure and better mechanical strength. The photothermal evaporation system composed of the hydrogel of the present invention has remarkable photothermal purification ability in brine and dye wastewater, and has broad application prospects in seawater desalination, sewage treatment and other fields.
Claims20
A preparation method of a gel, comprising:
- Step 1, add 2-10 mg/ml dopamine hydrochloride solution to 0.2-1 wt % ammonia solution to prepare dopamine aqueous solution, and add 0.1-0.5 g carnauba to 100 ml limonene to prepare carnauba wax solution, and prepare agar aqueous solution;
- Step 2, heat the agar aqueous solution prepared in step 1, then pour it into a polystyrene mold and cool it down to room temperature to form a gel, place the gel at 4° C. for 24 hours to age the gel, then freeze it in liquid nitrogen for 3-6 hours, and then place the gel at −18° C. for 12 hours to prevent cracking due to excessive temperature difference, and then thaw at room temperature;
- Step 3, soak the thawed gel prepared in step 2 in the dopamine aqueous solution for 24hours, and in-situ polymerize dopamine on the surface of the gel to generate a light-to-heat conversion material polydopamine;
- Step 4, soak the gel obtained in step 3 in an ethanol solution to change liquid;
- Step 5, soak the gel obtained in step 4 in the carnauba wax solution, and then dry it under normal pressure to obtain photothermal aerogel.
2 more elements
Dependencies are inferred from the claim text.