Back to results
US 12,741,882 B2Granted
Manufacture of titanium dioxide structures
AssigneeTiotech AS
InventorsRobert Corkery, Andreas Westermoen, Anders Teigland, Hjørdis Skår, Andre Marcel Bienfait
Life of this patent
Estimating the term…
Abstract
The present invention relates to a method for manufacturing a structure of a titanium compound selected from the group consisting of sheets, wires and tubes. The present invention also relates to intermediate products and structures comprising titanium dioxide obtainable by the method. The invention provides an improved method giving improved yield as well as other advantages.
Claims12
A method for manufacturing a structure of a titanium compound selected from the group consisting of sheets, wires and tubes, the method comprising
- ab) providing a dispersion of particles comprising TiO2, wherein the average diameter of the particles in the dispersion is 3-20 nm, and wherein the dispersion comprises citric acid,
- wherein the dispersion after step ab) comprises at least 15 wt % TiO2,
- c) adjusting the concentration of hydroxide ions in the dispersion from step ab) to at least 8 M by adding an alkali metal hydroxide MOH,
- d) treating the dispersion from step c) at a temperature in the interval 90-170° C. during 6-72 hours to obtain a plurality of first structures comprising alkali metal titanate, and
- e) treating the plurality of first structures comprising alkali metal titanate to exchange at least a part of the alkali metal ions M+ with H+ to obtain a plurality of second structures comprising protonated titanate.
2 more elements
Dependencies are inferred from the claim text.