Method for high-value application of PTA residue high-concentration bromine-containing wastewater to preparation of cuprous bromide

Abstract

The disclosure discloses a method for high-value application of PTA residue high-concentration bromine-containing wastewater to preparation of cuprous bromide, belongs to the field of PTA residue treatment, and includes: firstly adjusting a pH value of the bromine-containing wastewater to 0.5-2, adding cuprous oxide in batches, taking a reaction for 3-20 min after the cuprous oxide is totally added to produce cuprous bromide, Solid liquid separation to obtain cuprous bromide, concentrating a liquid phase to recover inorganic salt while rest wastewater may be used as process water for application. By cuprous oxide addition and method regulation and control, a bromine removal rate is as high as 95% or higher, the cuprous bromide reaches yield of 90% or higher and purity of 95%. Meanwhile, sodium sulfate with the purity of 90% or higher may be obtained. High-value application of the PTA residue high-concentration bromine-containing wastewater is really realized.

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