Fabrication of benzoxazine functionalized particles
AssigneeXerox Corporation
InventorsGabriel Iftime, Junhua Wei, Mahati Chintapalli
Life of this patent
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Abstract
A method includes adding particles to an alkaline solution, stirring the solution to cause the particles to acquire hydroxyl groups producing activated particles, dispersing the activated particles into a solvent solution, adding acetylene benzoxazine into the solvent solution, mixing the solvent solution, removing the solvent from the solvent solution to produce acetylene-benzoxazine functionalized particles, and drying the acetylene-benzoxazine functionalized particles. A composition of matter has acetylene-benzoxazine functionalized particles dispersed in a resin.
Claims15
A method, comprising:
- adding silicon carbide particles to an alkaline solution;
- stirring the alkaline solution to cause the silicon carbide particles to acquire hydroxyl groups producing activated silicon carbide particles;
- dispersing the activated silicon carbide particles into a solvent solution;
- adding acetylene benzoxazine into the solvent solution;
- mixing the solvent solution;
- removing the solvent from the solvent solution to produce acetylene-benzoxazine functionalized particles;
- drying the acetylene-benzoxazine functionalized silicon carbide particles;
- and
- mixing a mixture of the acetylene-benzoxazine functionalized silicon carbide particles with a benzoxazine monomer;
- initiating polymerization of the benzoxazine monomer in the mixture to create a resin having the acetylene-benzoxazine functionalized silicon carbide particles dispersed within;
- and
- curing the resin;
- wherein the solvent is one or more selected from the group consisting of:
- dichloromethane, chloroform, 1,1-dichloroethane, 1,2-dichloroethane, trichloro ethane, tetrahydrofuran, dioxane, ethylene glycol ethers, dimethyl glycol ethers, ethyl glycol ethers, diethylene glycol, and triethylene glycol.
Dependencies are inferred from the claim text.