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US 12,729,125 B2Granted
Production of metal borates with nano-dimension
AssigneeCelal Bayar Universitesi Tekn. Gel. Bol. A. S.
InventorsYuksel Abali, Osman Agus, Osman Arslan
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Abstract
A metal borate production method is realized by the reaction, M(NO3)+Na2B4O7·10H2O→M·B2O3·nH2O+NaNO3+nH2O, between borax and perchlorate or nitrate solution comprising a metal, or another completely dissolved metal salt in stochiometric proportion and the synthesis of nano-structured metal borates having antibacterial characteristic without addition of a second solvent or additive substance to the medium.
Claims5
A metal borate production method comprising a reaction between borax and a metal perchlorate;
- wherein the metal borate production method is realized in a stoichiometric proportion and a synthesis of nano-structured metal borates having antibacterial characteristic without addition of a second solvent or additive substance to a reaction medium, and comprises the following steps:
- adjusting reactive amounts of a metal perchlorate and a borax compound to be at a value between 1:1 and 2:1 by mole in a manner compliant to a reaction stoichiometry;
- adding the borax compound to the metal perchlorate with adjusted amounts and applying a mixing process at a value between 25 rpm and 250 rpm;
- conducting the reaction for at least 2 hours at a fixed temperature to obtain precipitation;
- applying washing, filtration and drying processes to the precipitation obtained as a result of the reaction to obtain a final product;
- and
- applying a sintering process the final product between temperatures 400° C. and 1500° C.
4 more elements
Dependencies are inferred from the claim text.