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US 12,721,345 B2Granted
Ultrafine gold nanocomposite, and preparation method and use thereof
AssigneeInnovation Center of Yangtze River Delta, ZJU
InventorsTian Ding, Mofei Shen, Jinsong Feng, Xinyu Liao, Yunlei Xianyu, Meimei Guo, Pengfei Ge
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Abstract
Provided are an ultrafine gold nanocomposite, and a preparation method and use thereof. The preparation method of the ultrafine gold nanocomposite includes the following steps: mixing a cyclodextrin metal-organic framework (CD-MOF) material, chloroauric acid and a solvent to obtain a mixture, and subjecting the mixture to incubation to obtain the ultrafine gold nanocomposite.
Claims11
A method for preparing an ultrafine gold nanocomposite, comprising the following steps:
- mixing a cyclodextrin metal-organic framework (CD-MOF) material, chloroauric acid and a solvent to obtain a mixture;
- and
- subjecting the mixture to incubation to obtain the ultrafine gold nanocomposite;
- wherein
- the method further comprises, before the mixing, preparing the CD-MOF material by:
- mixing γ-cyclodextrin (γ-CD), an alkali metal compound, water and an organic solvent to obtain a mixed material;
- and subjecting the mixed material to coordination to obtain a coordination product liquid;
- and
- mixing the coordination product liquid and a surfactant to obtain an admixture;
- and subjecting the admixture to crystallization to obtain the CD-MOF material;
- and
- an amount of the CD-MOF material is based on an amount of the γ-CD;
- a molar ratio of the γ-CD to the chloroauric acid is in a range of 5:1 to 7.5:1;
- and a ratio of an amount of substance of the chloroauric acid to a volume of the solvent is in a range of 1.25 mmol:
- 1 L to 1.5 mmol:
- 1 L.
13 more elements
Dependencies are inferred from the claim text.