Method of purifying phosphorus compound and method of reusing the same
AssigneeMaruzen Petrochemical Co., Ltd.
InventorYuta Saga
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Abstract
[Problem to be Solved] An object of the present invention is to provide a method of purifying a phosphorus compound, which method is capable of reducing the generation of a by-product during distillation. [Solution to Problem] The method of method of purifying a phosphorus compound according to the present invention includes the steps of: obtaining a mixture containing a specific phosphorus compound, a specific alkenyl phosphorus compound and a transition metal complex; and subjecting the resulting mixture to distillation after adding a Lewis acid to the mixture, to obtain a first distillate containing the specific phosphorus compound.
Claims10
A method of purifying a phosphorus compound, comprising the steps of:
- obtaining a mixture of a phosphorus compound represented by the following general formula (1):
- wherein, in general formula (1), each of R1 and R2 independently represents a substituted or unsubstituted alkyl group, a substituted or unsubstituted alkoxy group, a substituted or unsubstituted cycloalkyl group, a substituted or unsubstituted aralkyl group, a substituted or unsubstituted aryl group, or a substituted or unsubstituted aryloxy group;
- wherein R1 and R2 may be bonded with each other to form a cyclic structure, an alkenyl phosphorus compound represented by the following general formula (2):
- wherein, in general formula (2), the definitions of R1 and R2 are the same as those of R1 and R2 in the general formula (1) and a transition metal complex;
- and
- subjecting the mixture to distillation after adding a Lewis acid to the mixture, to obtain a first distillate containing the phosphorus compound represented by the general formula (1).
Dependencies are inferred from the claim text.