Method for the continuous preparation of formulated polyamide prepolymers
AssigneeArkema France
InventorsSébastien Quinebeche, Gérald Romazini, Pierrick Roger-Dalbert, Thierry Briffaud
Life of this patent
Estimating the term…
Loading patent…
AssigneeArkema France
InventorsSébastien Quinebeche, Gérald Romazini, Pierrick Roger-Dalbert, Thierry Briffaud
Estimating the term…
A method for continuously preparing a formulated polyamide prepolymer, of which the solution viscosity is from 0.25 dL/g to 0.70 dL/g, as measured according to ISO 307:2007 in m-cresol at 20° C., the method including a step of polycondensation on the basis of one or more polyamide precursor monomers, said polycondensation step being carried out in an extruder comprising at least two co-rotating conveying screws, the at least one monomer being previously fed therein in solid or liquid form without being dissolved in a solvent or in water, and said polycondensation step being carried out without extraction of the water formed during said polycondensation step and comprising the addition of at least one additive during said polycondensation step in the extruder.
A method for the continuous preparation of a formulated polyamide prepolymer, the formulated polyamide prepolymer having a viscosity in solution of which is comprised from 0.25 dL/g to 0.70 dL/g, as measured according to ISO 307:2007 in m-cresol at 20° C., said the formulated polyamide prepolymer having a weight average molecular weight (Mn) less than 10,000 g/mol as determined by calculation from the level of terminal functions determined by potentiometric titration in solution and the functionality of said the prepolymers or by NMR assay or by size exclusion chromatography,
Dependencies are inferred from the claim text.