Method for forming molybdenum carbide- containing nanocomposite electrode
AssigneeImam Abdulrahman Bin Faisal University
InventorsEmre Cevik, Ayhan Bozkurt
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Abstract
A nanocomposite electrode and a method of making the nanocomposite. The nanocomposite electrode includes an electrode substrate, nitrogen-doped molybdenum carbide nanosheets, at least one electrolyte, at least one binding compound, and at least one conductive additive. The electrode substrate is coated with a mixture of the nitrogen-doped molybdenum carbide nanosheets, at least one binding compound, at least one conductive additive, and at least one electrolyte, where the electrolyte penetrates the pores of the nitrogen-doped molybdenum carbide nanosheets, and where the nitrogen-doped molybdenum carbide nanosheets are an outer layer of the electrode.
Claims7
A method for forming a molybdenum carbide- containing nanocomposite electrode, comprising:
- forming nitrogen-doped molybdenum carbide nanosheets by:
- reacting an ammonium molybdate with an amino triazole in an ethanolic solution to form a reaction product;
- and
- calcining the reaction product under nitrogen;
- mixing at least one binding compound, at least one conductive additive, and at least one electrolyte to form a slurry;
- mixing the nitrogen-doped molybdenum carbide nanosheets with the slurry to form a synthesis mixture;
- coating the synthesis mixture onto a surface of an electrode substrate;
- and
- drying the nanocomposite electrode at a temperature less than 100° C. to form the nanocomposite electrode;
- wherein the nanocomposite electrode comprises:
- the electrode substrate;
- the nitrogen-doped molybdenum carbide nanosheets;
- the at least one electrolyte;
- the at least one binding compound;
- and
- the at least one conductive additive;
- wherein the electrolyte at least partially penetrates pores of the nitrogen-doped molybdenum carbide nanosheets;
- and
- wherein the nitrogen-doped molybdenum carbide nanosheets are an outer layer of the nanocomposite electrode.
Dependencies are inferred from the claim text.