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US 12,674,007 B2Granted
Preparation method for ethylene-vinyl alcohol copolymer
AssigneeLG Chem, Ltd.
InventorsHyojin Bae, Bongjune Kim, Sungjin Song, Se Won Baek
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Abstract
A method for preparing ethylene-vinyl alcohol copolymer capable of obtaining ethylene-vinyl alcohol copolymer of high saponification degree, while minimizing the amount of alkali catalysts used is disclosed herein. The method comprises adding a first alkali catalyst solution dropwise to ethylene-vinyl acetate copolymer dispersed in an alcohol solvent, and adding a second alkali catalyst solution dropwise to the first saponification reaction mixture.
Claims15
A method for preparing ethylene-vinyl alcohol copolymer, comprising:
- a first saponification reaction step wherein a first saponification reaction is performed while adding a first alkali catalyst solution dropwise to ethylene-vinyl acetate copolymer dispersed in an alcohol solvent, and a first saponification reaction mixture is obtained after the first saponification reaction step is completed;
- and
- a second saponification reaction step wherein a second saponification reaction is performed while adding a second alkali catalyst solution dropwise to the first saponification reaction mixture,
- wherein a total amount of the first alkali catalyst and second alkali catalyst used are 0.01 moles or more to less than 0.03 moles, based on 1 mole of vinyl acetate unit of the ethylene-vinyl acetate copolymer,
- the first saponification reaction step is completed when the dropwise addition of the first alkali catalyst solution is completed, and
- the second saponification reaction step is completed when the dropwise addition of the second alkali catalyst solution is completed.
3 more elements
Dependencies are inferred from the claim text.