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US 12,668,706 B2Granted
Antibacterial polymer composition
AssigneeLG Chem, Ltd.
InventorsJi Seok Lee, Hyungsam Choi, Seonjung Jung, Soonhee Kang, Haesung Yun
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Abstract
The present disclosure relates to an antibacterial polymer composition, and more particularly, to an antibacterial polymer composition that enables the preparation of a coating layer exhibiting excellent antibacterial properties.
Claims15
An antibacterial polymer composition comprising:
- a hydrophilic polymer;
- an antibacterial polymer that is a copolymer containing a repeating unit represented by Chemical Formula 1and a repeating unit represented by Chemical Formula 2;
- and
- a solvent containing water,
- wherein the antibacterial polymer composition has a viscosity under a constant temperature/humidity condition (23° C., 50% relative humidity) of 1,500 cP to 3,000 cP as measured using a Brookfield DV2T LV TJ0 viscometer with V-75 spindle at 200 rpm,
- wherein the antibacterial polymer composition has a bacterial growth inhibition rate against Proteus mirabilis of 60% or more as calculated by Equation 1:
- Bacterial
-
- growth
-
- inhibition
-
- rate
-
- (
- %
- )
- =
- (
- 1
- -
- A
- S
- A
- 0
- )
- ×
- 100
- [
- Equation
-
- 1
- ]
- wherein, As is an absorbance of an experimental group at 600 nm wavelength of Proteus mirabilis culture medium to which a sample is added, and A0 is an absorbance of a control group at 600 nm wavelength of the Proteus mirabilis culture medium to which the sample is not added,
- the experimental group is prepared by:
- applying the antibacterial polymer composition onto a release-treated PET film substrate so as to have a thickness of 200 μm using a bar coater, and then drying at 80° C. for 240 minutes to prepare an antibacterial film having a coating layer formed on one side of the substrate, and
- transferring 25 ml of broth type medium inoculated with Proteus Mirabilis at 3300 CFU/ml to a 50 mL conical tube, to which 0.1 g of the antibacterial film prepared is cut and added with alcohol-sterilized scissors, vortexing, and incubating in a shaking incubator at 37° C. for 16 hours, and
- the control group is prepared by culturing Proteus Mirabilis at 37° C. for 16 hours:
- in Chemical Formula 1,
- L is an alkylene having 1 to 10 carbon atoms,
- R1 to R3 are each independently hydrogen or methyl;
- one of R4 to R6 is an alkyl having 5 to 20 carbon atoms, and the rest of R4 to R6 are each independently an alkyl having 1 to 4 carbon atoms,
- X is halogen, and
- n is an integer of 10 to 10,000,
- in Chemical Formula 2,
- R′1 to R′3 are each independently hydrogen or methyl, and
- m is an integer of 1 or more.
44 more elements
Dependencies are inferred from the claim text.