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US 12,662,388 B2Granted
Control of an ammonia synthesis loop at partial load
AssigneeCasale SA
InventorMaurizio Rizzi
Life of this patent
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Abstract
A process for synthesis of ammonia wherein an ammonia synthesis loop includes an ammonia converter where a makeup gas is reacted to form ammonia, and the loop is controlled at a partial load by reducing the synthesis pressure and maintaining the reduced pressure within a desired range by controlling a bypass line of make-up gas of the converter.
Claims10
A process for synthesis of ammonia, the process comprising:
- producing an ammonia make-up synthesis gas in a front-end;
- raising the pressure of said make-up gas in a first compressor;
- feeding high-pressure make-up synthesis gas delivered by said first compressor to an ammonia synthesis loop;
- wherein said ammonia synthesis loop includes at least:
- a converter where ammonia is synthesized catalytically;
- a circulator, which is a compressor configured to maintain circulation in the loop and to deliver a feed gas, which includes the make-up synthesis gas, to said converter;
- a converter feed line from the circulator to the converter;
- a condensation section arranged downstream from the ammonia synthesis loop to receive an ammonia-containing gaseous product;
- and
- a separation section wherein a condensate produced in said condensation section is separated into an ammonia liquid product and a gaseous recycle stream;
- a recycle line from the separation section to a suction of the circulator;
- wherein the ammonia synthesis loop has a full load condition corresponding to the processing of a nominal flow rate of make-up gas transferred from the front end to the ammonia synthesis loop;
- and
- controlling the loop at a partial load condition, wherein the flow rate of make-up gas transferred from the front end to the loop is smaller than said nominal flow rate, by the following steps:
- the pressure at which ammonia is synthesized is lowered to a reduced ammonia synthesis pressure, which is less than a nominal synthesis pressure at said full load condition of the ammonia synthesis loop;
- and
- the synthesis pressure is maintained within a target range which includes said reduced synthesis pressure, by controlling a flow rate of feed gas bypassing the converter.
14 more elements
Dependencies are inferred from the claim text.