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US 12,655,084 B2Granted
Method for preparing an acrylic acid
AssigneeLG Chem, Ltd.
InventorsInho Choi, Hoiin Jeong, Yong O Im, Jiyoung Lee, Daeho Hong
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Abstract
The present disclosure relates to a method for preparing acrylic acid, and more particularly, to a method for preparing acrylic acid by dehydrating a lactic acid molecule through different steps with different temperatures. According to the preparation method of the present disclosure, acrylic acid can be prepared from lactic acid with a high conversion rate and yield, and also energy consumption can be further reduced as compared with a conventional method.
Claims12
A method for preparing acrylic acid, comprising the steps of:
- a first step of supplying an aqueous lactic acid solution to a reactor using a carrier gas;
- a second step of vaporizing the aqueous lactic acid solution to obtain vaporized lactic acid;
- a third step of bringing the vaporized lactic acid into contact with a dehydration catalyst;
- and
- a fourth step of obtaining acrylic acid,
- wherein;
- the first to the fourth steps are performed using a reactor equipped with a single reaction tube and a heating unit;
- the single reaction tube comprises a supply unit to which the aqueous lactic acid solution is supplied, a vaporization unit that vaporizes the aqueous lactic acid solution, a catalyst unit that brings the vaporized lactic acid into contact with the dehydration catalyst;
- and a discharge unit that discharges the acrylic acid;
- a heating unit comprises a first heating unit that heats the vaporization unit in a shape wrapping the single reaction tube, a second heating unit that is discontinuous with the first heating unit and heats a boundary portion between the vaporization unit and the catalyst unit and a front end of the catalyst unit, and a third heating unit which is discontinuous with the second heating unit and heats the rear end of the catalyst unit;
- and
- temperatures of the second to the fourth steps are each independently adjusted by the heating unit;
- and
- a set temperature of the second heating unit is higher than a set temperature of the third heating unit.
11 more elements
Dependencies are inferred from the claim text.