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US 12,617,013 B2Granted
Silver powder and method of producing same
AssigneeDowa Electronics Materials Co., Ltd.
InventorsKaori Tokusada, Hikaru Hayashida
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Abstract
Provided are a silver powder having powder physical properties enabling reduction of volume resistivity after firing and a method of producing this silver powder. The silver powder has a tap density of 4.8 g/mL or more, a TAP/D50 value (value determined by dividing the tap density (g/mL) by the volume-based median diameter (μm)) of not less than 7 and not more than 15, and a specific surface area of not less than 0.75 m2/g and not more than 1.3 m2/g.
Claims1
A method of producing a silver powder comprising:
- a milling step of using a pneumatic mill to accelerate and mill a silver powder produced by a wet reduction method;
- and
- a classification step of classifying the silver powder, performed after the milling step, wherein
- the milling step is performed with the silver powder having a powder concentration during milling of 0.2 kg/m3 or less,
- the classifying is performed such that after the classification step, the silver powder has powder physical properties of:
- a tap density of 4.8 g/mL or more;
- a TAP/D50 value that is a value determined by dividing the tap density by volume-based median diameter, in units of μm, of not less than 7 and not more than 15;
- and
- a specific surface area of not less than 0.75 m2/g and not more than 1.3 m2/g,
- a milling device in the milling step, a classifying device in the classification step, and a collecting device are connected in series in this order,
- an exhaust ventilator is connected at a downstream side of the collecting device and performs suction such that silver powder that has been supplied to the milling device is pneumatically conveyed to the collecting device, and
- a powder concentration during pneumatic conveyance determined by dividing a supply rate of silver powder in the milling step by an airflow rate of the exhaust ventilator is 0.08 kg/m3 or less.
9 more elements
Dependencies are inferred from the claim text.