Method for producing compound
AssigneeNippon Shokubai Co., Ltd.
InventorsHiroki Wada, Masashi Mukae, Yasutaka Takemoto, Toyofumi Sakai
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AssigneeNippon Shokubai Co., Ltd.
InventorsHiroki Wada, Masashi Mukae, Yasutaka Takemoto, Toyofumi Sakai
Estimating the term…
The present invention provides a method capable of sufficiently reducing impurities with excellent separation efficiency even from a crystal-containing slurry that contains a low-purity mother liquor and has poor solid-liquid separation properties. The present invention relates to a method for producing a compound, the method including: a step of feeding a slurry containing crystals of the compound to a hydraulic wash column; a step of melting crystals in a crystal-containing circulation slurry discharged from the hydraulic wash column; and a step of returning a portion of a circulation liquid containing a melt obtained in the melting step to the hydraulic wash column, wherein the circulation liquid returned in the returning step in an amount of more than 30% by mass relative to 100% by mass of the melt serves as a washing liquid for crystals.
A method for producing a compound, the method comprising:
A purification apparatus that purifies crystals, the purification apparatus comprising:
Dependencies are inferred from the claim text.