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US 12,606,444 B2Granted
Method for manufacturing silica sol
AssigneeFujimi Incorporated
InventorsMasaaki Ito, Jun Shinoda, Keiji Ashitaka
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Abstract
A method for manufacturing a silica sol according to an embodiment of the present invention includes: a step of preparing a silica sol reaction liquid by hydrolyzing and polycondensing an alkoxysilane or a condensate thereof using an alkali catalyst in a solvent; and at least one of a step of concentrating the silica sol reaction liquid by an ultrasonic atomization separation method and a step of replacing the silica sol reaction liquid with water by the ultrasonic atomization separation method.
Claims12
A method for manufacturing a silica sol, the method comprising:
- preparing a silica sol reaction liquid by hydrolyzing and polycondensing an alkoxysilane or a condensate thereof using an alkali catalyst in a solvent;
- and
- at least one of:
- concentrating the silica sol reaction liquid by an ultrasonic atomization separation method;
- or
- replacing the silica sol reaction liquid with water by the ultrasonic atomization separation method,
- wherein the ultrasonic atomization separation method comprises:
- continuously supplying the silica sol reaction liquid to an ultrasonic atomization chamber from a reaction liquid tank,
- irradiating the silica sol reaction liquid is with ultrasonic waves upward from a bottom of the ultrasonic atomization chamber toward a liquid surface of the silica sol reaction liquid to generate a mist from the liquid surface of the silica sol reaction liquid;
- introducing a carrier gas into the ultrasonic atomization chamber to transfer the mist of the silica sol reaction liquid atomized in the ultrasonic atomization chamber into a separator, wherein the separator is a cyclone;
- and
- subjecting the mist to centrifugal force in the cyclone, wherein the mist is separated based on the mass of the mist, and wherein mist having a large particle size comprising water and a very small amount of silica particles moves to an inner surface of the cyclone and is discharged from a lower outlet and supplied to a reaction tank, and mist comprising the solvent and the alkali catalyst discharges from an upper outlet.
9 more elements
Dependencies are inferred from the claim text.