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US 12,600,114 B2Granted
Drying processes for composite films comprising polyvinyl acetal and polyvinyl ethylene acetal resins
AssigneeKuraray Europe GmbH
InventorsShinichi Muguruma, Hideki Oomoto
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Abstract
The present invention relates to drying processes for composite films comprising a polyvinyl acetal on a carrier as well as to composite films and polyvinyl acetal films obtained in such processes.
Claims17
A process for the manufacture of a composite film, said composite film comprising:
- i) a film A comprising a polyvinyl acetal and/or a polyvinyl ethylene acetal and, optionally, a plasticiser, and
- ii) a carrier film,
- said process comprising the following steps, in that order:
- a) providing a carrier film;
- b) coating one surface of the carrier film with a solution comprising a solvent, the polyvinyl acetal and/or polyvinyl ethylene acetal, and the optional plasticizer;
- c1) drying the composite film on roll support at a temperature from 25 to 90° C.;
- and
- d) performing one or more drying steps selected from a list consisting of the following steps:
- IR drying, UV drying, microwave drying, vacuum drying, roll supported drying at a temperature of more than 130° C. and less than 180° C., air floatation drying at a temperature of more than 130° C. and less than 180° C.;
- to obtain the composite film, wherein the film A has a surface roughness Rz of 0.1 μm to 3.0 μm, and wherein the carrier film has a surface roughness Rz of 1.0 μm to 10 μm on a surface in contact with the film A.
7 more elements
A composite film comprising
- i) a carrier film, and
- ii) a film A comprising a polyvinyl acetal and/or a polyvinyl ethylene acetal and, optionally, a plasticizer,
- wherein the film A has a surface roughness Rz of 0.1 μm to 3.0 μm, and wherein the carrier film has a surface roughness Rz of 1.0 μm to 10 μm on a surface in contact with the film A, and
- wherein film A has a total residual solvent content of below 2000 ppm as measured according to JIS K 5601 May 1.
1 more element
Dependencies are inferred from the claim text.