# US 12,595,182 B2 · Method for producing chemical-treated metal oxide powder

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- Number: US 12,595,182 B2
- Document ID: US12595182B2
- Status: Granted
- Kind: B2
- Application number: 17/638,931
- Filed: 2020-08-04
- Published: 2022-09-15
- Granted: 2026-04-07
- Earliest claimed: 2019-09-02
- Assignees: Tokuyama Corporation
- Applicants: Tokuyama Corporation
- Inventors: Tadaharu Komatsubara
- Web page: https://patentgrep.com/patent/US12595182B2

## CPC

- C01B 33/18: Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof (preparation of aerogels by dehydrating gels C01B33/158; treatment to enhance the pigmenting or filling properties C09C)
- C01P 2004/03: obtained by SEM
- C01P 2006/12: Surface area
- C01B: NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; {METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C}
- C01P: INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

## Abstract

Aggregation of metal oxide powder is appropriately reduced. A method for chemical treatment of metal oxide powder (M) includes: a heating step (S10) of introducing the metal oxide powder (M) into a preheated stirring vessel (110) and performing heating while stirring the metal oxide powder (M) with a stirring blade (140); and a mixing step (S20) of adding a chemical agent to the metal oxide powder (M) and mixing the metal oxide powder (M) and the chemical agent while stirring the metal oxide powder (M) and the chemical agent with the stirring blade (140), wherein a rotation speed of the stirring blade (140) is lower in the mixing step (S20) than in the heating step (S10).

## Claims

### Claim 1

A method for producing chemical-treated metal oxide powder, the method comprising:
a heating step of introducing metal oxide powder having a specific surface area of not less than 20 m2/g and not more than 40 m2/g into a stirring vessel which has been preheated to a temperature of not lower than 220° C., and, while stirring the metal oxide powder with a stirring blade, performing heating so that a temperature inside the stirring vessel which temperature has been decreased by the introduction of the metal oxide powder reaches the temperature of not lower than 220° C. again; and
a mixing step of, after the temperature inside the stirring vessel has reached the temperature of not lower than 220° C. again in the heating step, adding a chemical agent to the metal oxide powder and mixing the metal oxide powder and the chemical agent while stirring the metal oxide powder and the chemical agent with the stirring blade,
wherein a rotation speed of the stirring blade is lower in the mixing step than in the heating step, and P/(ρ·n) is more than 0.15 and less than 0.25 where P denotes a stirring power of a motor that rotates the stirring blade, p denotes a bulk density of the metal oxide powder, and n denotes the rotation speed of the stirring blade.

### Claim 2 (depends on 1)

The method according to claim 1, wherein the rotation speed of the stirring blade in the heating step is not less than 85 rpm and not more than 200 rpm, and the rotation speed of the stirring blade in the mixing step is not less than 40 rpm and not more than 75 rpm.

### Claim 3 (depends on 1)

The method according to claim 1, wherein the metal oxide powder is silica or composite metal oxide powder containing silica as a main component.

### Claim 4 (depends on 1)

The method according to claim 1, wherein the chemical agent is a surface treatment agent.