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US 12,590,055 B2Granted
Process for producing isocyanates
AssigneeBASF SE
InventorsKai Thiele, Jens Ferbitz, Torsten Mattke
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Abstract
The present invention concerns a process for the preparation of isocyanates and/or polyisocyanates by reacting the corresponding amines with phosgene in a reactor, where isocyanates are obtained from a mixture of amines in gaseous or liquid form and phosgene in gaseous form, wherein no liquid solvents are used in the feeding, mixing, reacting, cooling, separating and purifying steps of the process.
Claims17
Process for the preparation of isocyanates or polyisocyanates by reacting the corresponding amines with phosgene, comprising the steps of
- a) feeding a first reactant stream containing the amine in gaseous or liquid form into a reactor,
- b) feeding a second reactant stream containing the phosgene in gaseous form into said reactor,
- c) mixing and reacting said first and second reactant streams in said reactor to obtain a reaction mixture,
- d) cooling said reaction mixture by indirect heat transfer or by quenching with cooled reaction product to obtain a liquid reaction product,
- e) separating said cooled reaction mixture into a liquid reaction product containing isocyanate and a gaseous reaction product,
- f) purifying said liquid reaction product to obtain liquid isocyanate, and
- h) separating said gaseous reaction product into a first gaseous product stream essentially comprising HCl and a second liquid or gaseous product stream essentially comprising phosgene,
- wherein no liquid solvent is used in steps a) to f) and h).
5 more elements
Dependencies are inferred from the claim text.