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US 12,571,786 B2Granted
Method of manufacturing metal nanoparticle-oxide support complex structure based gas sensor
AssigneeKorea Advanced Institute of Science and Technology
InventorsWooChul Jung, Il-Doo Kim, Jun Kyu Kim, Ji-Soo Jang
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Abstract
Provided is a method of producing a metal nanoparticle-oxide support complex structure, in which metal nanoparticles uniform in size are evenly distributed on the surface of oxide supports. A gas sensor with improved gas sensing ability and durability may be provided by using the same.
Claims9
A method of producing a metal nanoparticle-oxide support complex structure, the method comprising:
- a step (step 1) of mixing a precursor of the metal nanoparticle with a precursor of the oxide support to form a first mixture and additionally mixing a mixture of graphene oxide and nanocellulose with the first mixture of the precursor of the metal nanoparticle and the precursor of the oxide support to form a second mixture, wherein the second mixture consists of the precursor of the metal nanoparticle, the precursor of the oxide support, graphene oxide, and nanocellulose;
- a step (step 2) of preparing a solid solution by calcining and sintering the second mixture of the step 1;
- and
- a step (step 3) of forming the metal nanoparticles on the surface of the oxide supports by heat-treating the solid solution of the step 2 in a reducing atmosphere,
- wherein the graphene oxide and the nanocellulose are removed through the step 2, and
- wherein the precursor of the metal nanoparticle is an iridium (Ir) salt, and the precursor of the oxide support is a tungsten (W) salt.
3 more elements
Dependencies are inferred from the claim text.