Method of preparing ferric phosphate from iron-containing waste

Abstract

A method of preparing ferric phosphate from iron-containing waste, including: step a) providing a ferric chloride-containing mixture solution obtained from acidolysis of iron-containing waste; step b) adjusting pH of the ferric chloride-containing mixture solution to satisfy 0<pH≤2 and Fe3+ concentration to 10-80 g/L with an alkaline compound and water, to obtain an iron source solution; step c) mixing and reacting the iron source solution obtained from the step b) with a solution of calcium dihydrogen phosphate in a molar ratio of P to Fe of 1:1-1.8, to obtain a slurry with a pH of 0.2-2; and step d) performing aging and crystal transformation on the slurry, to obtain ferric phosphate. A battery-grade ferric phosphate with high purity and good product quality can be obtained without the need for deep purification of raw materials.

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