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US 12,528,240 B2Granted
Extruded polyvinyl alcohol fibres and fibrous products
AssigneeAquapak IP Limited
InventorsJohn Williams, Sian Griffiths, Robert Ashworth, Jack Eaton
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Abstract
This invention relates to polyvinyl alcohol fibers, methods of making polyvinyl alcohol fibers and products manufactured from polyvinyl alcohol fibers. The invention relates particularly but not exclusively to products comprising extruded polyvinyl alcohol fibers, methods of making extruded polyvinyl alcohol fibers and products incorporating such fibers.
Claims12
A method of manufacture of a nonwoven product comprising polyvinyl alcohol fibers comprising:
- providing a polyvinyl alcohol composition comprising homopolymeric polyvinyl alcohol having a degree of hydrolysis of 88% to 98% or greater and a molecular weight in the range from 22,000 to 38,000;
- adding a plasticizer selected from the group consisting of:
- diglycerol, triglycerol, fructose, ribose, xylose, D-mannitol, triacetin, pentaerythritol, dipentaerythritol, methyl pentanediol, 1,2-propanediol, 1,4-butanediol, 2-hydroxy-1,3-propanediol, 3-methyl-1,3-butanediol, 3,3-dimethyl-1,2-butanediol, polyethylene glycol 300, polyethylene glycol 400, alkoxylated polyethylene glycol, caprolactam, tricyclic trimethylolpropane formal, rosin esters, erucamide, and mixtures thereof to the composition;
- adding a stabilizer selected from the group consisting of sodium stearate, potassium oleate, sodium benzoate, calcium stearate, stearic acid, dimethyl pentane diol, propionic acid and mixtures thereof to the composition;
- melting the polyvinyl alcohol composition at a temperature from 190° C. to 250° C.;
- extruding the melted polyvinyl alcohol composition to form an extrudate;
- forming the extrudate into molten polyvinyl alcohol fibers;
- drawing the molten polyvinyl alcohol fibers to form individual molten polyvinyl alcohol fibers or bundles of molten polyvinyl alcohol fibers;
- and
- allowing the molten polyvinyl alcohol fibers to solidify to form solid polyvinyl alcohol fibers or bundles of solid polyvinyl alcohol fibers.
7 more elements
Dependencies are inferred from the claim text.