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US 12,521,328 B2Granted
1,3-butylene glycol product
AssigneeDaicel Corporation
InventorsYasuteru Kajikawa, Yuki Teshima, Yuuichirou Hirai, Keisuke Ono, Midori Umehara, Tetsuro Nakanishi
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Abstract
Provided is a high-purity 1,3-butylene glycol product that is odorless and is unlikely to cause acid concentration increase over time in a state containing water. A 1,3-butylene glycol product, having, according to a gas chromatographic analysis performed under predetermined conditions, a peak area ratio of 100 ppm or lower appearing in a relative retention time ranging from 1.35 to 1.45, provided that the relative retention time for a peak of 1,3-butylene glycol is 1.0.
Claims12
A 1,3-butylene glycol product having
- a peak area ratio of 100 ppm or lower appearing in a relative retention time ranging from 1.35 to 1.45, provided that the relative retention time for a peak of 1,3- butylene glycol is 1.0, according to a gas chromatographic analysis performed under following conditions:
- Analytical Column:
- a column with dimethylpolysiloxane as a stationary phase, having a length of 30 m, an inner diameter of 0.25 mm, and a film thickness of 1.0 μm;
- Heating Conditions:
- heating from 80° C. to 120° C. at 5° C./min, then heating again to 160° C. at 2° C./min and maintaining for 2 minutes, and further heating to 230° C. at 10° C./min and maintaining at 230° C. for 18 minutes;
- Sample Introduction Temperature:
- 250° C.;
- Carrier Gas:
- helium;
- Column Gas Flow Rate:
- 1 mL/min;
- and
- Detector and Detection Temperature:
- a flame ionization detector (FID), 280° C.
11 more elements
Dependencies are inferred from the claim text.