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US 12,515,193 B2Granted
Method for isolating a heavy metal ion from an aqueous solution
AssigneeKing Fahd University of Petroleum and Minerals
InventorsKhalid Alhooshani, Kazeem O. Sulaiman, Muhammad Sajid
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Abstract
A sorbent device based on a porous membrane bag (e.g., porous propylene membrane bag) encapsulated alkaline-modified zeolite (e.g., alkaline-treated USY zeolite). A process for removing heavy metals, such as Cd(II), Cr(III), and Pb(II) from an aqueous solution or an industrial wastewater samples with the sorbent device is provided. A method for preparing the alkaline-modified zeolite is also described.
Claims14
A method of isolating a heavy metal ion from an aqueous solution, the method comprising:
- contacting the aqueous solution with a sorbent device to form an aqueous mixture comprising a heavy metal loaded sorbent device;
- removing the heavy metal loaded sorbent device from the aqueous mixture thereby obtaining a purified solution having a reduced concentration of the heavy metal ion compared to an initial concentration;
- treating the heavy metal loaded sorbent device with an acid to desorb the heavy metal;
- wherein the sorbent device comprises:
- an alkaline-treated zeolite;
- and
- a porous membrane bag encapsulating the alkaline-treated zeolite,
- wherein the alkaline-treated zeolite comprises an ultrastable Y (USY) zeolite comprising a molar ratio of Si to Al in a range of 15:1 to 25:1, a Brunauer-Emmet-Taylor (BET) surface area in a range of 680 to 750 m2/g, and an adsorption capacity in a range of 2 to 100 mg Cr(III) per gram, 1 to 75 mg Pb(II) per gram, and 0.4 to 50 mg Cd(II) per gram.
5 more elements
Dependencies are inferred from the claim text.