Method for producing 1,3-butylene glycol, and 1,3-butylene glycol product
AssigneeDaicel Corporation
InventorMasahiko Shimizu
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AssigneeDaicel Corporation
InventorMasahiko Shimizu
Estimating the term…
Provided is a method capable of yielding high-purity 1,3-butylene glycol having a very low content of a low boiling point component and a high initial boiling point, with a high recovery ratio. A reaction crude liquid containing 1,3-butylene glycol is subjected to product distillation to yield purified 1,3-butylene glycol, through dehydration including removing water by distillation and performing high boiling point component removal including removing a high boiling point component by distillation. A method for producing 1,3 butylene glycol, the method including: distilling a charged liquid having a water content of 1.2 wt. % or less in a product column for use in the product distillation under a condition of a reflux ratio of greater than 0.1; distilling off a liquid in which a low boiling point component is concentrated from above a charging plate; and extracting 1,3-butylene glycol from below the charging plate.
A method for producing 1,3-butylene glycol to yield purified 1,3-butylene glycol from a reaction crude liquid comprising 1,3-butylene glycol, the method comprising:
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