Method for producing 1,3-butylene glycol, and 1,3-butylene glycol product
AssigneeDaicel Corporation
InventorsMasahiko Shimizu, Satoshi Kusakabe, Ryuji Saitou
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AssigneeDaicel Corporation
InventorsMasahiko Shimizu, Satoshi Kusakabe, Ryuji Saitou
Estimating the term…
Provided is a method capable of yielding high-purity 1,3-butylene glycol having a very low content of a high boiling point component and a low dry point, with a high recovery ratio. A method for producing 1,3-butylene glycol to yield purified 1,3-butylene glycol from a reaction crude liquid containing 1,3-butylene glycol, in which, in a high boiling point component removal column for use in the removing a high boiling point component, a charged liquid containing 1,3 -butylene glycol is distilled under conditions that (i) a reflux ratio is greater than 0.02 in a case where a concentration of 1,3-butylene glycol in the charged liquid is 95% or less, or a reflux ratio is greater than 0.01 in a case where the concentration of 1,3-butylene glycol in the charged liquid is greater than 95%, and (ii) a bottom ratio of less than 30 wt. %, high-purity 1,3-butylene glycol is distilled off from above a charging plate, and a liquid in which a high boiling point component is concentrated is extracted from below the charging plate.
A method for producing 1,3-butylene glycol to yield purified 1,3-butylene glycol from a reaction crude liquid including 1,3-butylene glycol, the method comprising:
Dependencies are inferred from the claim text.