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US 12,466,799 B2Granted
Method for producing N,N-disubstituted benzthiazolyl-sulfenamides
AssigneeLANXESS Deutschland GmbH
InventorsHolger Graf, Melanie Wiedemeier-Jarad, Jörg Hagemann, Nele De Smet
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Abstract
The invention relates to a method for preparing N, N-disubstituted benzthiazolylsulfenamides.
Claims12
A method for preparing N, N-disubstituted benzothiazolylsulfenamides of the formula (I)
- where R1, R2=each independently —CH(R3)(R4)
- where R3, R4=each independently H, C3-alkyl,
- and R5=C1-C3-alkyl,
- y=0 to 2, and
- n=0 to 5,
- by reacting 2-mercaptobenzothiazole salts of the formula (II)
- where Z=Na or K,
- with amines of the formula (III)
- NH(R1)(R2) (III)
- in which R1 and R2 have the definition above,
- wherein the reaction is carried out in the presence of sodium hypochlorite at a pH of 10 to 12.
8 more elements
Dependencies are inferred from the claim text.