Method of producing phosphate-coated SmFeN-based anisotropic magnetic powder and phosphate-coated SmFeN-based anisotropic magnetic powder
AssigneeNichia Corporation
InventorsMasahiro Abe, Satoshi Yamanaka, Shuichi Tada, Kenta Iwai
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Abstract
A method of producing a phosphate-coated SmFeN-based anisotropic magnetic powder, the method including performing a phosphate treatment including adding an inorganic acid to a slurry containing a raw material SmFeN-based anisotropic magnetic powder, water, a phosphate compound, and a rare earth compound so that the slurry is adjusted to have a pH of at least 1 and not higher than 4.5 to obtain a phosphate-coated SmFeN-based anisotropic magnetic powder having a surface coated with a phosphate.
Claims17
A method of producing a phosphate-coated SmFeN-based anisotropic magnetic powder, the method comprising
- performing a phosphate treatment comprising adding an inorganic acid to a slurry containing a SmFeN-based anisotropic magnetic powder, water, a phosphate compound, and a rare earth compound containing a rare earth element so that the slurry is adjusted to have a pH of at least 1 and not higher than 4.5 to obtain a phosphate-coated SmFeN-based anisotropic magnetic powder having a surface coated with a phosphate, and
- after the phosphate treatment, heat-treating the phosphate-coated SmFeN-based anisotropic magnetic powder at a temperature of at least 150° C. but not higher than 330° C. in an oxygen-containing atmosphere,
- wherein the rare earth compound is at least one compound selected from the group consisting of a rare earth hydroxide, a rare earth chloride, a rare earth sulfate, a rare earth nitrate, a rare earth acetate, and a combination thereof, and
- wherein the solvent of the slurry is water.
A method of producing a phosphate-coated SmFeN-based anisotropic magnetic powder, the method comprising
- performing a phosphate treatment comprising adding an inorganic acid to a slurry containing a SmFeN-based anisotropic magnetic powder, water, a phosphate compound, and a rare earth compound containing a rare earth element so that the slurry is adjusted to have a pH of at least 1 and not higher than 4.5 to obtain a phosphate-coated SmFeN-based anisotropic magnetic powder having a surface coated with a phosphate, and
- after the phosphate treatment, heat-treating the phosphate-coated SmFeN-based anisotropic magnetic powder at a temperature of at least 150° C. but not higher than 330° C. in an oxygen-containing atmosphere,
- wherein the rare earth compound is at least one compound that can generate rare earth ions in a slurry containing water as a solvent, or a combination thereof, and
- wherein the solvent of the slurry is water.
Dependencies are inferred from the claim text.