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US 12,448,730 B2Granted
Preparation of cellulose fibers
AssigneeJena Trading Aps
InventorsPer Vinther, John Mark Lawther
Life of this patent
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Abstract
The present invention provides a method of producing an improved cellulose pulp consisting of cellulose fibers of a desired length, such as cellulose fibers having a length-weighted average fiber length Lc(l)>0.6 mm and its use in cellulose pulp-comprising products, such as packaging material with improved properties.
Claims13
A method of isolating and preparing cellulose fibers of a desired length-weighted average fiber length lc(l) from cereal straw, the method comprising:
- (i) subjecting the cereal straw to a pretreatment comprising a dry mechanical treatment to remove parts of the cuticular wax from the cereal straw followed by enzymatic pretreatment using one or more protease and/or pectinase enzymes in aqueous suspension to remove remaining cuticular wax from the cereal straw, thus obtaining a solution comprising dewaxed straw material in aqueous suspension,
- (ii) solubilizing hemicellulose and lignin components of the solution in (i) by adjusting the pH and increasing the temperature of the solution to pH 9-11.5 and temperature of 65-95° C. to provide a material,
- (iii) separating the material obtained in (ii) into a solid cellulose fiber fraction and a liquid fraction comprising solubilized hemicellulose and lignin components,
- (iv) suspending the solid cellulose fiber fraction obtained in (iii) in an aqueous liquid, adjusting the temperature and pH of the aqueous liquid to a temperature of 65-95° C. and pH 9-11.5, adding a bleaching agent, and keeping the cellulose fiber fraction in suspension for 60-180 minutes (T1) to provide a bleached material,
- (v) subjecting the bleached material obtained in (iv) to a wet mechanical refining treatment to provide a bleached-refined material,
- (vi) continuing bleaching at a temperature 65-95° C. and a pH 9-11.5 for a duration of 20-90 minutes (T3) without wet mechanical treatment,
- (vii) obtaining a cellulose fiber product by separating the bleached-refined material obtained in (vi) into a bleached-refined solid cellulose fiber fraction and an aqueous bleaching liquor fraction, and
- (viii) optionally washing the bleached-refined cellulose fiber fraction in an aqueous liquid,
- wherein the length-weighted fiber length lc(l) of the cellulose fibers is >0.6 mm.
6 more elements
Dependencies are inferred from the claim text.