Back to results
US 12,441,887 B2Granted
Partially saponified rice bran wax oxidates
AssigneeClariant International Ltd.
InventorsPhilipp Kratzer, Manuel Broehmer, Rainer Fell
Life of this patent
Estimating the term…
Abstract
The invention relates to partially saponified rice bran wax oxidates, to a process for the production of these products and to their use for agriculture or forestry purposes, as an additive in plastics processing, in care products, in printing inks and/or in paints.
Claims19
A process for producing a partly saponified rice bran wax oxidate (V), comprising the steps of:
- i) providing a rice bran wax (R) containing less than 20% by weight, based on the total weight of the rice bran wax (R), of polyesters formed from polyhydric alcohols and aliphatic carboxylic acids having 8 to 20 carbon atoms;
- ii) providing a mixture (M) of chromium trioxide and sulfuric acid;
- iii) performing the oxidation of the rice bran wax (R) by reacting the rice bran wax (R) with the mixture (M) while stirring at a temperature of 90 to 150° C., in order to obtain a reaction mixture containing rice bran wax oxidate (O);
- iv) ending the reaction and leaving the reaction mixture obtained in step iii) to stand until an organic phase has separated from an aqueous phase;
- v) separating off the organic phase;
- vi) optionally removing residues containing chromium compounds from the organic phase in order to obtain the rice bran wax oxidate (O) in purified form;
- vii) optionally repeating the sequence of steps ii) to vi) using the rice wax oxidate (O), optionally in purified form, rather than the rice bran wax (R);
- and
- viii) saponifying the rice bran wax oxidate (O), optionally in purified form, by reacting it with a basic salt,
- wherein no alcohol component is added to the reaction mixture in step iii) to step viii).
7 more elements
A partly saponified rice bran wax oxidate (V) comprising the following components:
- a) 30% to 85% by weight, based on the total weight of the partly saponified rice bran wax oxidate (V), of genuine esters having 42 to 64 carbon atoms;
- b) 0% to 70% by weight, based on the total weight of the partly saponified rice bran wax oxidate (V), of salts of aliphatic carboxylic acids having 8 to 36 carbon atoms;
- and
- c) 0% to 5% by weight, based on the total weight of the partly saponified rice bran wax oxidate (V), of polyesters formed from polyhydric alcohols and aliphatic carboxylic acids having 22 to 36 carbon atoms.
1 more element
Dependencies are inferred from the claim text.