Back to results
US 12,331,200 B2Granted
Production of surface-reacted calcium salts by grinding induced conversion
AssigneeOmya International AG
InventorsDaniel E. Gerard, Lassi Karvonen
Life of this patent
Estimating the term…
Abstract
The present invention relates to a process for producing an aqueous suspension of surface-reacted calcium salt particles by mixing a calcium salt excluding monocalcium phosphate and dicalcium phosphate, a calcium phosphate selected from monocalcium phosphate and/or dicalcium phosphate, with water, and grinding the obtained aqueous suspension at a pH value of at least 4.2 to form an aqueous suspension of surface-reacted calcium salt particles.
Claims12
A process for producing an aqueous suspension of surface-reacted calcium salt particles comprising the steps of:
- a) providing a calcium salt excluding monocalcium phosphate and dicalcium phosphate,
- b) providing a calcium phosphate, wherein the calcium phosphate is dicalcium phosphate and is produced by contacting a calcium ion source and a phosphate ion source,
- c) forming an aqueous suspension by mixing the calcium salt of step a), and the calcium phosphate of step b) with water, and
- d) grinding the aqueous suspension of step c) at a pH value from 4.2 to 14 and at a temperature of 0° C. to 100° C. to form an aqueous suspension of surface-reacted calcium salt particles,
- wherein the calcium salt of step a) and the calcium phosphate of step b) in combination have a calcium ion to a phosphate ion molar ratio (Ca2+:
- PO43−) in the range from 2.2:1 to 100:1;
- wherein grinding of step d) is carried out:
- (1) in a ball mill, a rod mill, a vibrating mill, a centrifugal impact mill, a vertical bead mill, an attrition mill, a sand mill, or combinations thereof;
- and
- (2) at a specific grinding energy from 50 to 500 kWh per dry metric ton of (2) surface-reacted calcium salt particles.
7 more elements
Dependencies are inferred from the claim text.