Fine grain structures for tough rare earth permanent magnets
AssigneeIowa State University Research Foundation, Inc.
InventorsBaozhi Cui, Jun Cui
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AssigneeIowa State University Research Foundation, Inc.
InventorsBaozhi Cui, Jun Cui
Estimating the term…
The present invention provides fine grain structures for rare earth permanent magnets (REPMs) and their production in a manner to significantly enhance flexural strength and fracture toughness of the magnets with no or little sacrifice in the hard magnetic properties. The tough REPMs can have either homogeneous or heterogeneous refined grain microstructural architectures achieved by introducing a small amount of additive particle materials into the magnet matrix, such as fine-sized, insoluble, chemically stable, and non-reactive with the magnet matrix. These additive materials can act effectively as both heterogeneous nuclei sites and grain growth inhibitors during the heat treatment processes, which in turn resulting in refined grain structures of the REPMs. Alternatively, the fine grain structures were also achieved by using magnet alloy feedstock powders with finer particle sizes. The fine grains acting as the strengthening sites can inhibit the crack nucleation and can also slow down the propagation of micro-cracks, which in turn increasing magnet's fracture toughness.
A sintered rare earth permanent magnet comprising at least one region comprised of a sintered feedstock blend of rare earth alloy feedstock particles and artificially-added grain-refining submicron feedstock particles having an average particle size of less than 1 micron wherein the sintered feedstock blend provides a refined grain microstructure that includes a rare earth alloy magnet matrix and the artificially-added grain-refining submicron feedstock particles dispersed in the microstructure which has an average refined grain size from about 15 to less than 40 microns, wherein the at least one region having the refined grain microstructure provides the sintered magnet with at least one of mechanical toughness and/or mechanical strength beneficial for inhibiting micro-cracking of the magnet.
A sintered rare earth permanent magnet comprising at least one region having a refined grain microstructure that includes a microstructure matrix and artificially-added grain-refining, submicron feedstock particles selected from at least one of carbide particles, fluoride particles, nitride particles, oxide particles, and/or sulfide particles dispersed in the mircostructure where they are non-reactive and insoluble without alteration of the matrix chemical composition and where the grain-refining submicron feedstock particles have an average particle size of less than 1 micron in the microstructure which has an average refined relatively fine grain size of about 22 to about 32 microns, wherein the at least one region having the refined grain microstructure provides the sintered magnet with at least one of mechanical toughness and/or mechanical strength beneficial for inhibiting micro-cracking of the magnet.
Dependencies are inferred from the claim text.