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US 12,269,931 B2Granted
Polymer based sensors for detecting agricultural analytes and methods of making same
AssigneeGeorgia Tech Research Corporation
InventorsJie Xu, Douglas Britton
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Abstract
A polymer-based sensor for detecting agricultural analytes is disclosed, including stable polymer-based sensing films such as molecular imprinted polymers (MIPs) that can be incorporated in sensors for detecting herbicides and pesticides, as well as methods of making the sensing films.
Claims13
A method of preparing a molecularly imprinted polymer in the form of a xerogel film for detecting one or more agricultural analytes, the method comprising:
- preparing a mixture of precursors comprising:
- a crosslinking organosilane;
- a functional organosilane;
- water;
- and
- an acid or a base;
- dissolving one or more agricultural analytes in one or more porogens to form an agricultural analyte solution;
- mixing the mixture of precursors and the agricultural analyte solution with a cross-linker and, optionally, a catalyst until a sol forms;
- coating the sol on a pre-cleaned sensor to form a coated sol;
- drying the coated sol to transform the coated sol into a xerogel film;
- and
- flowing a porogen over the xerogel film to remove the one or more agricultural analytes thereby forming a molecularly imprinted polymer in the form of a xerogel film.
9 more elements
Dependencies are inferred from the claim text.