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US 12,215,063 B2Granted
Method for preparing deuterated compound
AssigneeLG Chem, Ltd.
InventorsSunmin Kim, Wanpyo Hong, Woochul Lee, Kyung Seok Jeong, Woo Han Kim
Life of this patent
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Abstract
A method for preparing a deuterated compound, and a composition including the deuterated compound are provided. The method comprises preparing a compound of Chemical Formula 2 by reacting a compound of Chemical Formula 1; a deuterium source; and a metal catalyst, and forming a compound of Chemical Formula 3 by using the compound of Chemical Formula 2:
Claims8
A method for preparing a deuterated compound, the method comprising:
- preparing a compound of Chemical Formula 2 by reacting a compound of Chemical Formula 1;
- a deuterium source;
- and a metal catalyst, and
- forming a compound of Chemical Formula 3 reacting the compound of Chemical Formula 2,
- wherein in Chemical Formulae 1 to 3,
- R1 is hydrogen;
- a cyano group;
- a nitro group;
- a halogen group;
- a hydroxyl group;
- a substituted or unsubstituted alkyl group;
- a substituted or unsubstituted cycloalkyl group;
- a substituted or unsubstituted aryl group;
- or a substituted or unsubstituted heteroaryl group,
- R2 is hydrogen or deuterium,
- R3 is hydrogen;
- deuterium;
- a substituted or unsubstituted alkyl group;
- a substituted or unsubstituted cycloalkyl group;
- a substituted or unsubstituted aryl group;
- or a substituted or unsubstituted heteroaryl group,
- Ar1 and Ar2 are the same as or different from each other, and each independently a substituted or unsubstituted aryl group;
- or a substituted or unsubstituted heteroaryl group,
- L1 is a direct bond;
- a substituted or unsubstituted arylene group;
- or a substituted or unsubstituted heteroarylene group,
- D is deuterium,
- r1 is an integer of 0 to 8, r1′ is an integer of 0 to 4, r1″ is an integer of 0 to 3, and when r1, r1′ and r1″ are 2 or greater, R1s are the same as or different from each other,
- r3 is an integer of 0 to 8, and when r3 is 2 or greater, R3s are the same as or different from each other, and
- n1 is an integer of 1 to 5, and n2 is an integer of 1 to 4.
27 more elements
Dependencies are inferred from the claim text.