# US 12,181,458 B2 · Fiber-optic bundle for in-situ spectral sensor, spectral sensor and method of making and using the same

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- Number: US 12,181,458 B2
- Document ID: US12181458B2
- Status: Granted
- Kind: B2
- Application number: 18/086,219
- Filed: 2022-12-21
- Published: 2024-06-27
- Granted: 2024-12-31
- Earliest claimed: 2022-12-21
- Assignees: LandScan LLC
- Applicants: LandScan LLC
- Inventors: Neal Edward Van Wyck; Darren C. Nolet; Maxwell S. Farrington; Stephen P. Farrington; Daniel James Rooney
- Web page: https://patentgrep.com/patent/US12181458B2

## CPC

- G01N 33/24: Earth materials (G01N33/42 takes precedence)
- G01J 3/0208: {using focussing or collimating elements, e.g. lenses or mirrors; performing aberration correction}
- G01J 3/0218: {using optical fibers}
- G01J 3/0291: {Housings; Spectrometer accessories; Spatial arrangement of elements, e.g. folded path arrangements}
- G01J 3/108: {for measurement in the infrared range}
- G01J 3/42: Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry (beam switching arrangements G01J3/08)
- G01N 33/245: {for agricultural purposes}
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- G01J: MEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY (light sources F21, H01J, H01K, H05B; investigating properties of materials by optical means G01N)

## Abstract

Fiber-optic bundles for infrared spectral analysis of media. The fiber-optic bundles can be used in infrared probes configured to be inserted in media for in-situ characterization of the media. The fiber-optic bundles can include a plurality of optical fibers arranged in a spatial pattern at a sampling end of the bundle to improve a signal of infrared spectral measurements. In-situ probes of the present disclosure can be used for precision farming practices to improve soil health and increase crop yields.

## Claims

### Claim 1

A fiber-optic bundle, comprising:
a sampling end; and
a plurality of optical fibers that include:
a first receiver fiber;
a second receiver fiber; and
a plurality of illumination fibers arranged in an asymmetric pattern at the sampling end, wherein the asymmetric pattern is designed and configured to provide a first illumination intensity incident on the first receiver fiber and a second illumination intensity incident on the second receiver fiber, wherein the first illumination intensity is greater than the second illumination intensity.

### Claim 2 (depends on 1)

The fiber-optic bundle of claim 1, wherein the asymmetric pattern includes a circular arrangement of a first group of the illumination fibers and the second receiver fiber and the first receiver fiber located in the middle of the circular arrangement.

### Claim 3 (depends on 2)

The fiber-optic bundle of claim 2, wherein the asymmetric pattern further includes a second group of the illumination fibers positioned outside of the circular arrangement and directly adjacent the second receiver fiber.

### Claim 4 (depends on 3)

The fiber-optic bundle of claim 3, wherein a number of the illumination fibers in the first group of illumination fibers is greater than a number of the illumination fibers in the second group of illumination fibers.

### Claim 5 (depends on 1)

The fiber-optic bundle of claim 1, wherein the asymmetric pattern includes a round pattern that includes a first group of the illumination fibers and the second receiver fiber positioned in an annular space envelope and the first receiver fiber located in the middle of the annular space envelope, wherein the illumination fibers include a second group of fibers located at least partially radially outside of the annular space envelope.

### Claim 6 (depends on 1)

The fiber-optic bundle of claim 1:
wherein a sampling end of the first receiver fiber and a sampling end of the second receiver fiber are positioned in a receiver fiber plane;
wherein the sampling end of the first receiver fiber is located on a first side of a second plane and the sampling end of the second receiver fiber is located on a second side of the second plane, wherein the second plane is perpendicular to the receiver fiber plane;
wherein each of the plurality of illumination fibers includes a sampling end, wherein a total surface area of the sampling ends of the plurality of illumination fibers located on the first side of the second plane is greater than a total surface area of the sampling ends of the plurality of illumination fibers located on the second side of the second plane.

### Claim 7 (depends on 1)

The fiber-optic bundle of claim 1, wherein the first receiver fiber is configured to be connected to an infrared spectrometer and configured to transmit at least one of near-infrared or mid-infrared light and the second receiver fiber is configured to be connected to a visible light spectrometer and configured to transmit visible light.

### Claim 8 (depends on 7)

The fiber-optic bundle of claim 7, wherein the first receiver fiber has at least one of a different chemical composition, different core diameter, or different construction than the second receiver fiber.

### Claim 9 (depends on 7)

The fiber-optic bundle of claim 7, wherein a core material of the first receiver fiber has a lower concentration of hydroxyl groups than a core material of the second receiver fiber.

### Claim 10 (depends on 1)

The fiber-optic bundle of claim 1, wherein the first illumination intensity and the second illumination intensity are each an intensity of diffusely reflected light reflected by media.

### Claim 11 (depends on 10)

The fiber-optic bundle of claim 10, wherein the diffusely reflected light travels along an optical path in an in-situ spectral probe, the optical path including a window and a mirror.

### Claim 12 (depends on 1)

The fiber-optic bundle of claim 1, further comprising a sampling head located at the sampling end, wherein the sampling head includes a fixture having a contoured inner wall having a shape that is complementary to a shape of an outer extent of the plurality of optical fibers for holding the plurality of optical fibers in a desired spatial arrangement during assembly of the fiber-optic bundle.

### Claim 13 (depends on 12)

The fiber-optic bundle of claim 12, wherein the shape of the inner wall includes a plurality of elongate portions each having an arcuate cross sectional shape.

### Claim 14 (depends on 1)

A system, comprising:
a soil probe;
a fiber-optic bundle according to claim 1 disposed in the soil probe; and
a mirror located in the soil probe adjacent the sampling end of the fiber-optic bundle.

### Claim 15 (depends on 14)

The system of claim 14, wherein the first receiver fiber is configured to be connected to an infrared spectrometer and the second receiver fiber is configured to be connected to a visible light spectrometer, further wherein the mirror has a mirror surface that is positioned at an acute angle with respect to a central longitudinal axis of the sampling end of the fiber-optic bundle.

### Claim 16 (depends on 15)

The system of claim 15, wherein a distance between a sampling end of the first receiver fiber and the mirror surface is substantially the same as a distance between a sampling end of the second receiver fiber and the mirror surface.

### Claim 17 (depends on 15)

The system of claim 15, wherein a distance between a sampling end of the first receiver fiber and the mirror surface is less than a distance between a sampling end of the second receiver fiber and the mirror surface.

### Claim 18 (depends on 15)

The system of claim 15, wherein a distance between a sampling end of the first receiver fiber and the mirror surface is greater than a distance between a sampling end of the second receiver fiber and the mirror surface.

### Claim 19 (depends on 15)

The system of claim 15, further comprising an infrared (IR) spectrometer, a visible light (VIS) spectrometer, and a light source, further wherein the fiber-optic bundle includes a common portion that extends from the sampling end to a fiber leg junction and a plurality of legs that include a first leg that extends from the fiber leg junction to the IR spectrometer, a second leg that extends from the fiber leg junction to the VIS spectrometer, and a third leg that extends from the fiber leg junction to the light source, wherein a length of at least one of the plurality of legs is different than a length of the other legs.

### Claim 20 (depends on 19)

The system of claim 19, wherein the third leg is connected to the light source by a connector, wherein the connector is a commercial off the shelf connector that has been modified to increase an internal diameter of the connector to maximize a total cross sectional area of core diameters of the plurality of illumination fibers.
