# US 12,180,107 B2 · Methods for producing a hollow-core fiber and for producing a preform for a hollow-core fiber

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- Number: US 12,180,107 B2
- Document ID: US12180107B2
- Status: Granted
- Kind: B2
- Application number: 17/621,607
- Filed: 2020-07-15
- Published: 2022-11-10
- Granted: 2024-12-31
- Earliest claimed: 2019-07-17
- Assignees: Heraeus Quarzglas GmbH & Co. KG
- Applicants: Heraeus Quarzglas GmbH & Co. KG
- Inventors: Manuel Rosenberger; Enrico Ehrentraut; Benjamin Reis; Yusuf Tansel; David Kostka; Ralph Sattmann; Jan Vydra
- Web page: https://patentgrep.com/patent/US12180107B2

## CPC

- C03B 37/02781: {Hollow fibres, e.g. holey fibres}
- C03B 37/0122: {for making preforms of photonic crystal, microstructured or holey optical fibres}
- C03B 37/01234: {to form longitudinal grooves, e.g. by chamfering}
- C03B 2203/14: Non-solid, i.e. hollow products, e.g. hollow clad or with core-clad interface
- C03B 2203/16: Hollow core
- C03B 2203/42: Photonic crystal fibres, e.g. fibres using the photonic bandgap PBG effect, microstructured or holey optical fibres
- C03B: MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES

## Abstract

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that a positioning template is inserted into the cladding tube inner bore in order to arrange the anti-resonant element preforms, said template having holding elements for positioning the anti-resonant element preforms at the target positions.

## Claims

### Claim 1

A method for producing an anti-resonant hollow-core fiber having a hollow core extending along a longitudinal axis of the hollow-core fiber and an inner sheath surrounding the hollow core, which sheath includes a plurality of anti-resonance elements, the method comprising the steps of:
(a) providing a cladding tube having an inner bore and a longitudinal axis, along which a cladding tube wall delimited by an inner side and an outer side extends;
(b) providing a plurality of anti-resonance element preforms;
(c) arranging the anti-resonance element preforms at desired positions on the inner side of the cladding tube wall to form a primary preform for the hollow-core fiber by inserting a positioning template having holding elements into the inner bore of the cladding tube so that the holding elements position the anti-resonance element preforms at the desired positions; and
(d) elongating the primary preform to form the hollow-core fiber, or further processing the primary preform into a secondary preform from which the hollow-core fiber is drawn, wherein the further processing includes a single or repeated performance of one or more of the following hot-forming processes:
(i) elongating the primary preform,
(ii) collapsing the primary preform,
(iii) collapsing and simultaneously elongating the primary preform,
(iv) collapsing additional sheath material,
(v) collapsing additional sheath material and subsequently elongating the primary preform,
(vi) collapsing additional sheath material and simultaneously elongating the primary preform, wherein the positioning template has at least one latch which interacts with a counterpart latch in the cladding tube wall to form a force-fitting and/or positive-locking connection.

### Claim 2 (depends on 1)

The method according to claim 1, wherein the positioning template has a shaft projecting into the inner bore of the cladding tube, which shaft has a plurality of holding arms pointing radially outwards.

### Claim 3 (depends on 1)

The method according to claim 1, wherein the anti-resonance element preforms are tubular with an outer tube surface, and each holding element has at least two points of contact with the outer tube surface of the anti-resonance element preform that is to be held.

### Claim 4 (depends on 1)

The method according to claim 1, wherein the cladding tube has a pair of end faces and the positioning template is used in the region of at least one of the end faces.

### Claim 5 (depends on 1)

The method according to claim 1, wherein the counterpart latch is arranged in an end face of the cladding tube wall and the latch is completely retractable therein.

### Claim 6 (depends on 1)

The method according to claim 1, wherein the counterpart latch does not extend as far as an outer face of the cladding tube.

### Claim 7 (depends on 1)

The method according to claim 1, wherein the positioning template consists of graphite or glass.

### Claim 8 (depends on 1)

The method according to claim 1, further comprising producing the positioning template by machining with a dimensional deviation of less than +/−0.1 mm.

### Claim 9 (depends on 1)

The method according to claim 1, wherein the cladding tube has a circular inner cross-section and the inner side of the cladding tube wall has a longitudinal structure that is designed as a longitudinal groove or as a longitudinal slot.

### Claim 10 (depends on 1)

The method according to claim 1, further comprising machining the inner side of the cladding tube.

### Claim 11 (depends on 1)

The method according to claim 1, further comprising fixing and/or sealing using a sealing or bonding compound containing amorphous SiO2 particles to arrange the anti-resonance element preforms at the desired positions on the inner side of the cladding tube wall and/or to elongate or further process the primary preform according to method step (d).

### Claim 12

A method for producing a preform for an anti-resonant hollow-core fiber having a hollow core extending along a longitudinal axis of the hollow-core fiber and an inner sheath surrounding the hollow core, which sheath includes a plurality of anti-resonance elements, the method comprising the steps of:
(a) providing a cladding tube having an inner bore and a longitudinal axis, along which a cladding tube wall delimited by an inner side and an outer side extends;
(b) providing a plurality of anti-resonance element preforms;
(c) arranging the anti-resonance element preforms at desired positions on the inner side of the cladding tube wall to form a primary preform for the hollow-core fiber by inserting a positioning template having holding elements into the inner bore of the cladding tube so that the holding elements position the anti-resonance element preforms at the desired positions; and
(d) optionally further processing the primary preform into a secondary preform for the hollow-core fiber, wherein the further processing includes a single or repeated performance of one or more of the following hot-forming processes:
(i) elongating the primary preform,
(ii) collapsing the primary preform,
(iii) collapsing and simultaneously elongating the primary preform,
(iv) collapsing additional sheath material,
(v) collapsing additional sheath material and subsequently elongating the primary preform,
(vi) collapsing additional sheath material and simultaneously elongating the primary preform, wherein the positioning template has at least one latch which interacts with a counterpart latch in the cladding tube wall to form a force-fitting and/or positive-locking connection.

### Claim 13 (depends on 12)

The method according to claim 12, wherein the positioning template has a shaft projecting into the inner bore of the cladding tube, which shaft has a plurality of holding arms pointing radially outwards.

### Claim 14 (depends on 12)

The method according to claim 12, wherein the positioning template has holding elements and the anti-resonance element preforms are tubular with an outer tube surface, and each holding element has at least two points of contact with the outer tube surface of the anti-resonance element preform that is to be held.

### Claim 15 (depends on 12)

The method according to claim 12, wherein the cladding tube has a pair of end faces and the positioning template is used in the region of at least one of the end faces.

### Claim 16 (depends on 4)

The method according to claim 4, wherein the positioning template is used in the region of both of the end faces.

### Claim 17 (depends on 7)

The method according to claim 7, wherein the positioning template consists of quartz glass.

### Claim 18 (depends on 10)

The method according to claim 10, wherein the step of machining includes drilling, milling, grinding, honing, and/or polishing.

### Claim 19

A method for producing an anti-resonant hollow-core fiber having a hollow core extending along a longitudinal axis of the hollow-core fiber and an inner sheath surrounding the hollow core, which sheath includes a plurality of anti-resonance elements, the method comprising the steps of:
(a) providing a cladding tube having an inner bore, a pair of end faces, and a longitudinal axis, along which a cladding tube wall delimited by an inner side and an outer side extends;
(b) providing a plurality of tubular anti-resonance element preforms with an outer tube surface;
(c) arranging the anti-resonance element preforms at desired positions on the inner side of the cladding tube wall to form a primary preform for the hollow-core fiber by inserting a positioning template having holding elements into the inner bore of the cladding tube so that the holding elements position the anti-resonance element preforms at the desired positions, wherein the positioning template has a shaft that projects into the inner bore of the cladding tube and has a plurality of holding arms pointing radially outwards, each holding element has at least two points of contact with the outer tube surface of the anti-resonance element preform that is to be held, and the positioning template is used in the region of at least one of the end faces; and
(d) elongating the primary preform to form the hollow-core fiber, or further processing the primary preform into a secondary preform from which the hollow-core fiber is drawn, wherein the further processing includes a single or repeated performance of one or more of the following hot-forming processes:
(i) elongating the primary preform,
(ii) collapsing the primary preform,
(iii) collapsing and simultaneously elongating the primary preform,
(iv) collapsing additional sheath material,
(v) collapsing additional sheath material and subsequently elongating the primary preform,
(vi) collapsing additional sheath material and simultaneously elongating the primary preform, wherein the positioning template has at least one latch which interacts with a counterpart latch in the cladding tube wall to form a force-fitting and/or positive-locking connection.
