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US 12,133,777 B2Granted
Zirconia sintered body, zirconia composition, zirconia pre-sintered body and dental prosthesis
AssigneeKuraray Noritake Dental Inc.
InventorsYoshihisa Yamada, Atsushi Matsumoto, Yoshihisa Ito
Life of this patent
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Abstract
A zirconia pre-sintered body suitable for dental milling, grinding and/or cutting can provide a sintered body in which the strength between layers of powders is improved. A flexural strength of a test sample of the zirconia sintered body, measured pursuant to JISR1601, is preferably not less than 1000 or 1100 MPa.
Claims5
A zirconia pre-sintered body configured for dental milling, grinding, and/or cutting, the body comprising a plurality of pre-sintered layers,
- wherein the zirconia pre-sintered body has a flexural strength of a test sample of the zirconia pre-sintered body, measured pursuant to JISR1601, is not less than 90% of the flexural strength of a comparative zirconia pre-sintered body,
- wherein the test sample being formed by:
- preparing a plurality of zirconia powders, each comprising zirconia and yttria as a stabilizer that suppresses phase transition of zirconia, the plurality of zirconia powders differing in composition,
- laminating the plurality of zirconia powders to form a plurality of zirconia powder layers;
- vibrating the zirconia powder layers to produce interlayer boundary portions having compositional mixtures of respective zirconia powders of respective adjacent pairs of the plurality of zirconia powder layers;
- and
- pre-sintering the plurality of zirconia powder layers to form the zirconia pre-sintered body;
- wherein as a result of sintering, each of the plurality of zirconia powders becomes a respective one of the layers of the plurality of pre-sintered layers, the interlayer boundary portions of the plurality of sintered layers having a gradient of the compositional mixture of each of the respective adjacent pairs of the plurality of sintered layers,
- wherein the comparative zirconia pre-sintered body is formed by pre-sintering one composition of the plurality of zirconia powders alone at the same temperature as a pre-sintering temperature of the test sample, and
- wherein the flexural strength of the test sample is measured under a condition that a load point of a three-point bending test is positioned at a position of an interlayer boundary of the pre-sintered layers, the interlayer boundary traversing the test sample of the pre-sintered body along a direction of load application.
7 more elements
A zirconia pre-sintered body configured for dental milling, grinding, and/or cutting, the body comprising a plurality of pre-sintered layers,
- wherein the zirconia pre-sintered body has a flexural strength of a test sample of the zirconia pre-sintered body, measured pursuant to JISR1601, is not less than 90% of the flexural strength of a comparative zirconia pre-sintered body,
- wherein the test sample being formed by:
- preparing a plurality of zirconia powders, each comprising zirconia and yttria as a stabilizer that suppresses phase transition of zirconia, the plurality of zirconia powders differing in composition,
- laminating the plurality of zirconia powders to form a plurality of zirconia powder layers;
- and
- pre-sintering the plurality of zirconia powder layers to form the zirconia pre-sintered body;
- wherein as a result of sintering, each of the plurality of zirconia powders becomes a respective one of the layers of the plurality of pre-sintered layers, interlayer boundary portions of the plurality of sintered layers having a gradient of the compositional mixture of each of the respective adjacent pairs of the plurality of sintered layers,
- wherein, in direction traversing the plurality of sintered layers, a b* color chromaticity value is non-constant and increases constantly in a direction traversing the plurality of sintered layers, including the interlayer boundary portions,
- wherein the comparative zirconia pre-sintered body is formed by pre-sintering one composition of the plurality of zirconia powders alone at the same temperature as a pre-sintering temperature of the test sample,
- wherein the flexural strength of the test sample is measured under a condition that a load point of a three-point bending test is positioned at a position of an interlayer boundary of the pre-sintered layers, the interlayer boundary traversing the test sample of the pre-sintered body along a direction of load application, and
- wherein the plurality of zirconia powders comprise at least one pigment in different ratios, respectively.
8 more elements
Dependencies are inferred from the claim text.